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GCMS reanalysis note for sample AE08264, May 6 2002

Machine-extracted title · confidence 100%

Laboratory comment noting low recovery in initial GCMS scan of sample AE08264, resulting in re-extraction.

NYC-WTC_000044338–000044348

Folder label: “GCMS X 4/23/02 A 4/26/02

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Scanned page image, NYC-WTC_000044341
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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\l\DATA\MAY0102\8264.D Vial: 3 Acq On 1 May 2002 9:55 am Operator: Sample gc/ms scan 4/23 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 1 10:52 2002 Quant Results File: GCMS0501.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed May 01 10:40:31 2002 Response via : Initial Calibration DataAcq Meth : GCMS0501

Compound R.T. Qlon Response Cone Unit Qvalue

35) Anthracene 25.59 178 307 N.D. 36) Di-n-butylphthalate 27.55 149 11456 0.30 ug/1 # 98 37) Fluoranthene 0.00 202 0 N.D. 39) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 32.08 149 496 N.D. 41) Benzo(a)anthracene 33.64 228 2195 N.D. 42) Bis(2-ethylhexyl)phthalate 33.86 149 6355 0.38 ug/1 99 43) Chrysene 33.72 228 523 N.D. 45) Di-n-Octylphthalate 35.59 149 458 N.D. 46) Benzo(b)fluoranthene 36.70 252 278 N.D. 47) Benzo(k)fluoranthene 36.77 252 471 N.D. 48) Benzo(a)pyrene 37.69 252 319 N.D. 49) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 8264.D GCMS0501.M Wed May 01 11:40:45 2002 Page 2

NYC-WTC_000044341

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NYC-WTC_000044341Source: NYC Law Department, mirrored locally

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