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GCMS calibration data for sample AE07484, April 2002

Machine-extracted title · confidence 90%

Calibration record for GCMS analysis using standard compounds, generated on April 19, 2002, to ensure instrument accuracy.

NYC-WTC_000044279–000044288

Folder label: “GCMS X 4/23/02 A 4/26/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\APR1802\7484.D Vial: 17 Acq On : 20 Apr 2002 9:11 am Operator: Sample : gc/ms scan 4/1 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 22 12:20 2002 <Quant Results File: GCMS0419.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0419.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Apr 19 14:51:24 2002 Response via : Initial Calibration DataAcq Meth : GCMS0412

Compound R.T. Qlon Response Cone Unit Qvalue' 33) Hexachlorobenzene 0.00 284 0 N.D. 34) Phenanthrene 25.65 178 1246 N.D. 35) Anthracene 25.78 178 1132 N.D. 36) Di-n-butylphthalate 27.55 149 6279 N.D. 37) Fluoranthene 29.27 202 1466 N.D. 4 0) Pyrene 29.95 202 1304 N.D. 41) Butylbenzylphthalate 32.08 149 1572 N.D. 42) Benzo(a)anthracene 33.59 228 18498 0.67 ug/1 97 43) Bis(2-ethylhexyl)phthalate 33.86 149 16416 0.66 ug/1 98 44) Chrysene 33.71 228 36538 1.34 ug/1 99 46) Di-n-Octylphthalate 35.60 149 9510 N.D. 47) Benzo(b)fluoranthene 36.69 252 18024 0.70 ug/1 99 48) Benzo(k)fluoranthene 36.75 252 29930 1.19 ug/1 94 49) Benzo(a)pyrene 37.68 252 8956 0.42 ug/1 # 87 50) Indeno(1,2,3-cd)pyrene 41.95 276 11507 0.53 ug/1 95 51) Dibenz(a,h)anthracene 42.02 278 9121 0.56 ug/1 # 87 52) Benzo(g,h,i)perylene 43.17 276 11862 0.66 ug/1 95

(#) = qualifier out of range (m) = manual integration 7484.D GCMS0419.M Mon Apr 22 12:24:58 2002 Page 2

NYC-WTC_000044280

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NYC-WTC_000044280Source: NYC Law Department, mirrored locally

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