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GCMS analysis results for sample AE07484, May 2002

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of sample AE07484 conducted on May 6, 2002, including surrogate recovery data.

NYC-WTC_000044268–000044278

Folder label: “GCMS X 4/23/02 A 4/26/02

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Scanned page image, NYC-WTC_000044273
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\l\DATA\APR2502\7484.D Vial: 7 Acq On : 26 Apr 2002 11:15 pm Operator: Sample : gc/ms scan 4/23 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.187 338 342 371 rVB 283719 739104 22.09% 4.418% 2 12.208 775 780 794 rVB 949420 2285757 68.32% 13.662% 3 12.447 802 806 814 rBV 19272 47623 1.42% 0.285% 4 15.844 1170 1176 1191 rBV 1430891 2919463 87.26% 17.450% 5 21.141 1747 1753 1774 rBV 1578925 3345890 100.00% 19.999%

6 23.280 1979 1986 1993 rBV 215093 431132 12.89% 2.577% 7 25.584 2230 2237 2248 rBV2 1548968 3163708 94.56% 18.910% 8 25.722 2248 2252 2262 rVB2 12643 36681 1.10% 0.219% 9 33.635 3108 3114 3133 rBV2 961816 2209980 66.05% 13.209% 10 37.867 3567 3575 3589 rBV2 533127 1551163 46.36% 9.271%

Sum of corrected areas: 16730501

7484.D GCMS0412.M Thu May 02 05:34:17 2002

NYC-WTC_000044273

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NYC-WTC_000044273Source: NYC Law Department, mirrored locally

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