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GCMS calibration results for sample AE09334, April 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS calibration data for sample AE09334 generated on April 25-26, 2002.

NYC-WTC_000046351–000046359

Folder label: “GCMS X 5/7/02 A 5/9/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\APR2502\9334.D Vial : 11 Acq On : 25 Apr 2002 10:26 pm Operator: Sample : gc/ms scan 4/18 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.187 338 342 347 rBV 276610 542694 10.37% 2.035% 2 8.252 347 349 367 rVB 34799 117468 2.24% 0.440% 3 12.208 775 780 796 rVB 1603677 3585052 68.49% 13.443% 4 15.844 1170 1176 1193 rBV 2257894 4587456 87.64% 17.201% 5 21.150 1747 1754 1775 rBV 2510567 5234510 100.00% 19.627%

6 23.280 1980 1986 1993 rBV 204520 406060 7.76% 1.523% 7 25.593 2230 2238 2248 rBV 2351109 5101158 97.45% 19.127% 8 25.722 2248 2252 2264 rVB 19802 58008 1.11% 0.218% 9 33.644 3108 3115 3134 rBV2 1687136 3926911 75.02% 14.724% 10 33.855 3134 3138 3152 rVB2 49056 123932 2.37% 0.465%

11 37.876 3567 3576 3593 rBV2 981855 2986136 57.05% 11.197%

Sum of corrected areas: 26669385

9334.D GCMS0412.M Fri Apr 26 08:19:09 2002

NYC-WTC_000046354

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NYC-WTC_000046354Source: NYC Law Department, mirrored locally

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