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← Document results/DEP Box 25/GCMS X 4/25/02 A 5/7/02
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GCMS analysis results, sample AE09972, May 2002

Machine-extracted title · confidence 100%

Laboratory report for sample AE09972 showing surrogate recovery and unknown compounds from May 9, 2002.

NYC-WTC_000044001–000044024

Folder label: “GCMS X 4/25/02 A 5/7/02”

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Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\050602\9972.D Vial: 20 Acq On 7 May 2002 3:11 am Operator: Mclean Sample 4/25 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 6 1-Hexene, 4,5-dimethyl- Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

4.95 0.39 ug/L 313663 1,4-Dichlorobenzene-d4 9.94

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Hexene, 4,5-dimethyl- 112 C8H16 016106-59-5 50 2 3-Penten-2-ol 86 C5H10O 001569-50-2 50 3 3-Buten-2-ol, 2-methyl- 86 C5H10O 000115-18-4 42 4 3-Penten-2-ol 86 C5H10O 001569-50-2 40 Abundance Scan 318 (4.948 min): 9972. D (-313) (-) m/z 71.10 ‘'100.00% 71 43

5000 55 I A 85 ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' 1 ' 37 4.60 4.80 5.00 5.20 H +8L — | M , , | I li + r " 1 r 1" i'' " i — I I I I I I I I I I ■ | । i i i | I I I I | i i i i । । m/ z 43.10 78.00%

U m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #6302: 1 -Hexene, 4,5-dimethyl- 43 71 WwPwhAV 5000 55 i । l । । । [l m । ] i i-! । । । । । । । f

4.60 4.80 5.00 5.20 27 m/z 41.05 53.06% s ■ 1! 11 ■ ■ ■ ■ । ■ 50 I. , 65 15 ‘ i1' " i I | r i i i [ I 1 H f4 r i i ITTTTrt 77 84 97 I । । । । । । r । r r 11 । > । । । । । 11 । । । । । । । ' 11 । । ।

mlz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #114531: 3-Penten-2-ol

43 71 wAtow b/vuuoy I I | I I I i [ I I I I I I I > I I I I Tf"(l

4.60 4.80 5.00 5.20 5000 m/z 55.10 32.15%

27 53 co 86 i "'1 r " • i 41,32.7.38, I lI 11 I I I I I I111111581111 I 65, I [ I 11 I I +T [ 1 1 I I I I I I I [ I I I r I I I I I I I I I I f

m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #114557: 3-Buten-2-ol, 2-methyl- 1 1 i 1 ■ ' 1 i 1 ' 1 1 r ‘ ' ' i 1 1 1 1 i ' 71 4.60 4.80 5.00 5.20_____ 43 m/z 69.10 27.62%

5000 59

27 I 36 1111111,53 86 1111111 - I I I I I I I I I I I I I ' I I I I I I I I j I At 1 1 1 + 54+4 I I I | I I I I | I I I > [ I !!) | I I I I | I I I I | I I I I | I 1 ................ [ I I I [ I I r ...................... I I I I I | ) I t I | | r

m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 4.60 480 5.00 5.20

9972.D 050102.M Tue May 07 15:50:58 2002 Page 10

NYC-WTC_000044015

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GCMS analysis results, sample AE09968, May 2002 · Box DEP Box 25

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Gas chromatography-mass spectrometry analysis report for sample AE09968, detecting unknown compounds and 2,4-DDD surrogate with 78% recovery, dated May 9, 2002.

1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997

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