GCMS analysis results, sample AE09970, May 2002

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Laboratory report for sample AE09970 showing surrogate recovery and unknown compounds from May 9, 2002.

NYC-WTC_000043976–000044000

Folder label: “GCMS X 4/25/02 A 5/7/02”

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Data File C:\MSDCHEM\1\DATA\050602\9970.D Vial: 27 Acq On 7 May 2002 8:52 am Operator: Mclean Sample 4/25 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\l\METHQDS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 15 1-Butanamine Concentration Rank 14 R.T. EstConc Area Relative to ISTD R.T. 35.00 0.24 ug/L 143610 Perylene-dl2 34.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Butanamine 73 C4H11N 000109-73-9 3 2 1-Butanamine 73 C4H11N 000109-73-9 3 3 N-Ethylformamide 73 C3H7NO 000627-45-2/3 4 1-Butanamine 73 C4H11N 000109-73/9 3 Abundance Scan 5432 (34.995 min): 9970.D (-5431) (-) m/z 40.10 100.00% 43 WMMMW

5000

73 262 !dT 132 207 34.60 34.80 35.00 35.20 35.40

m/z-->20 .............. 40 60 I.,80 100 120 140 160 180 200 220 240 260 ------- m/z 73.10 21.92%! Abundance #108150: 1-Butanamine

.1111II 33

5000 | I I । I| I 11 I I I I I I I T f |

34.60 34.80 35.00 35.20 35.40 73 m/z 262.20 18.17% 18 .I J 1, 12,56.......................................... 1 । | > । । l| । । li । । । । । । । । । । | । i i r-|-i-r r-r-]" i-i i i । i i i i । t i i i । i i r i ] CUUrFr m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #108242:1-Butanamine 33 I i i > । । i r । F | I i i i । । i i i—j—i-r

34.60 34.80 35.00 35.20 35.40 5000 m/ z 49.00 15.33%|

. 73 ,42 56 1. ..................................................... 1 । | । । । TI । । r । । । । । । । । । । । । । । । । ] 1 । । । । । । । । । । r "i ■ । । m । i i । i j-i i i i । i ।

m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #857: N-Ethylformamide 33 34.60 34.80 35.00 35.20 35.40 73 m/z 50.90 12.75%

5000 44 58 18 1.1 H- 1 1 ■ 1 i 1 r'"") ’ ।" r i i ll । । । । i i ri । । । । । [ i th i ] i i i । । i । i । । i i i । [ i r ■ ' ! 1 1 1 1 i 1 /z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 34.60 34.80 35.00 35'20 35.40

9970.D 050102.M Tue May 07 15:49:51 2002 Page 19

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GCMS analysis results, sample AE09973, May 2002 · Box DEP Box 25

NYC-WTC_000044025

Laboratory report for sample AE09973 showing surrogate recovery and unknown compounds from May 9, 2002.

1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998