Gas chromatography-mass spectrometry analysis report for sample AE09968, detecting unknown compounds and 2,4-DDD surrogate with 78% recovery, dated May 9, 2002.
NYC-WTC_000043938–000043957Folder label: “GCMS X 4/25/02 A 5/7/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\MSDCHEM\1\DATA\050602\9968.D Vial : 25 Acq On 7 May 2002 7:14 am Operator: Mclean Sample 4/25 Inst : Instrumen Misc : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L
Peak Number 3 2-Butene, 1-methoxy-, (Z)- Concentration Rank 4
R.T. EstConc Area Relative to ISTD R.T.
5.64 0.43 ug/L 308117 1,4-Dichlorobenzene-d4 9.94
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 2-Butene, 1-methoxy-, (Z) - 86 C5H10O 010034-16-9 53. 2 Furan, tetrahydro-2-methyl- 86 C5H10O 000096-47-943 3 l-Hexene, 4,5-dimethyl- 112 C8H16 016106-59-5 28 4 2-Butyn-I-ol, 4-methoxy- 100 C5H802 018857-03-9 25 Abundance Scan 436 (5.641 min): 9968.D (-427) (-) m/z 41.20 100.00% 41 71
5000
35 53 59 86 ——P — S 5.20 5.40 5.60 5.80 6.00 TT r "11" 1' r1" i ■ 48 I 1 I 1 I I I I I I I I I I I 1 I | 1 1 1 T ' n" 1 ' ' ITT’ I | H >> | > i I I | I । I I | I 1 1 । | r m/z 43.10 97.30% m/z->____ 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #24227: 2-Butene, 1-methoxy-, (Z)- 71
41 27 5000 55 5.20 5.40 5.60 5.80 6.00 86 m/z 71.10 80.39% 50 । 60 66 ,33 , ‘1T r 111 r "' r "' J HH , i n । h " |, — 11111~ । FIpultr I' 11" " |l1 " 11'
/z—>____5 10 15 20 25 30 35 40 45 _50 55 60 65 70 75 80 85 90 95 100105 Abundance #109891: Furan, tetrahydro-2-methyl- 43 71
5.20 5.40 5.60 5.80 6.00 5000 27 m/z 39.20 50,. 34% 56
m/z-> 5 l-rp pill 15 +2,—4 — 38 51 I —MT 86
10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 m Abundance #6302: 1-Hexene, 4,5-dimethyl- । । fnf *| । । f/fi । । r . 43 5.20 5.40 5.60 5.80 6.00 71 m/z 69.10 38.99%
5000 55
27
v 15 i" " r1" i ! ! | I H । L 11159.1 I I । । । i m651111 I 77 84 97 I | I | I I I I | । | I I | । I r > | i i I i | I I I I | I i r i | < ........ I I I I I I I I I ‘ I , T T i । i , I 1 I i r
m/z~> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 5.20 5.40 5.60 5.80 6.00
9968.D 050102.M Tue May 07 15:47:02 2002 Page 7
NYC-WTC_000043949
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Ranked by indexed similarity. Reasons describe shared subjects and filing context; check the source records.
NYC-WTC_000043958
Laboratory report for sample AE09969 showing surrogate recovery and unknown compounds from May 9, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043919
Laboratory report for sample AE09967 showing surrogate recovery and unknown compounds from May 9, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044926
Laboratory report showing gas chromatography-mass spectrometry results for unidentified organic compounds in sample AE10199 on May 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043976
Laboratory report for sample AE09970 showing surrogate recovery and unknown compounds from May 9, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044994
Laboratory report showing gas chromatography-mass spectrometry results for unidentified organic compounds in sample AE10204 on May 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044071
Laboratory report for sample AE09971 showing surrogate recovery and unknown compounds from May 9, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045171
Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE10308 conducted on May 17, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044885
Laboratory report showing gas chromatography-mass spectrometry results for unidentified organic compounds in sample AE10198 on May 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044001
Laboratory report for sample AE09972 showing surrogate recovery and unknown compounds from May 9, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045137
Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE10306 conducted on May 17, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045155
Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE10307 conducted on May 17, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045075
Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE10303 conducted on May 17, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000043745
Single-page administrative log from DEP Box 25 covering GCMS X analyses dated between April 25 and May 7, 2002.
Filed in the same folder
NYC-WTC_000043746
Fragmented page containing Method 508 headers and partial text from a DEP laboratory record dated April 2002.
Filed in the same folder
NYC-WTC_000043749
Laboratory report documenting a method blank analysis for GC/MS testing of volatile organic compounds from May 2002.
Filed in the same folder
NYC-WTC_000043756
Calibration data report for sample AE09684 listing response factors and concentrations for target analytes in May 2002.
Filed in the same folder
NYC-WTC_000043760
Reference gas chromatography-mass spectrometry analysis with manual result entry for sample AE09684, detecting multiple organic contaminants.
Filed in the same folder