GCMS analysis results, sample AE08016, May 2002

NYC 9/11 Public Portal Document

Data File C:\HPCHEM\1\DATA\MAY0602\8016.D Vial: 26 Acq On 7 May 2002 4:47 pm Operator: Sample GC/MS SCAN 4/25 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.16 7.42 ug/1 676178 1,4-Dichlorobenzene-d4 12.19

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pent/none, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 64 2 CH2=CMCH2C(O)OCH3 100 C5H802 003724-55-8 9 3 5-Hexen-2-one 98 C6H10O 000109-49-9 7 000067-64-1 7 4 Acetone 58 C3H60 Abundance Scan 341 (8.162 min): 8016. D (-) m/z 43.05 100.00% 43

5000 59 I । | । I- 1 I [ I i I i | I i i 7 । । I I l l 101 780 8.00 8.20 8.40 8.60 53 , 69 83 , | 1—i—। । । । । । i rn i | r1 1 38 i i r 1 :—| ! rr — I-1 I I | I I I I | I ' I I I-1 I-! I I pi I I I | I m/z 59.10 42.46% m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #64274: 2-Pentanone, 4-hydroxy-4-methyl- 43

■ 1 r1 1 7 1 |1 I 11 | J I I I | ! 1.1 I [ 5000 59 780 8.00 8.20 8.40 8.60 m/ z 58.10 16.53% 27 101

m/z—>10 ........................... II ' 1 i ' 1 1 ' i 1 1 ' ' I 20 30 — 40 4950—+ 60 1 I 1 ’ 1 kkkkk,i ■ 1 1 1 I 70 80 83 90 - 100 110 Abundance #1448: CH2=CHCH2C(O)OCH3 43 7.80 8.00 8.20 8.40 8.60 5000 m/ z 101.15 13.21%

58 I 72 100 1 ■ i 1 ' ' 1 i ' 1 1 1 । 38,4 i ' '। i 1 ' 1 1 i ' 11 m/z->10 20 30 40 50 60 70 80 90 100 110 Abundance #63205: 5-Hexen-2-one 43 7.80 8.00 8.20 8.40 8.60 m/z 41.15 6.87%

5000

55 15 27 .......... | 1 1 I ‘ 1 1 1 I —384 I I 50 I 1 i'll I nki I I" I I I-—I I [ 1 83 1 —I m 98 d I I I 11 I I - r A i r [ i H । । । r r * — I | I- m/z— > 10 20 30 40 50 60 70 80 90 100 110 7.80 8.00 8.20 8.40 8.60

8016 .D GCMS0501.M Thu May 09 11:24:58 2002 Page 1

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