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← Document results/DEP Box 25/GCMS X 4/24/02 A 5/3/02
Document / 15 pages

GC/MS calibration table, sample AE08837, April 2002

Machine-extracted title · confidence 90%

Calibration data for GC/MS analysis of surrogate compounds including dichlorobenzenes and naphthalene from April 2002.

NYC-WTC_000043699–000043713

Folder label: “GCMS X 4/24/02 A 5/3/02”

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OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document LDU ALEc ELCEIL KCDOL L

Data File : C:\HPCHEM\1\DATA\APR2302\8837.D Vial: 6 ‘ Acq On : 23 Apr 2002 7:18 pm Operator: Sample : gc/ms scan 4/15 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 6.285 130 135 153 rBV 347410 835865 20.05% 3.492% 2 6.551 160 164 179 rVB 37658 97566 2.34% 0.408% 3 7.258 237 241 248 rBV 29568 59742 1.43% 0.250% 4 7.726 287 292 305 rBV2 43954 110633 2.65% 0.462% 5 8.185 339 342 347 rW 361039 710514 17.05% 2.968%

6 8.250 347 349 373 rVB 64065 225549 5.41% 0.942% 7 9.149 443 447 474 rVB 413218 1087089 26.08% 4.541% 8 9.663 495 503 522 rBV 117409 359581 8.63% 1.502% 9 9.966 532 536 550 rBV2 34207 103104 2.47% 0.431% 10 12.206 775 780 797 rVB 1169292 2868693 68.83% 11.984%

11 14.813 1059 1064 1069 rBV 72041 138475 3.32% 0.579% 12 15.842 1170 1176 1194 rBV 1794602 3690434 88.54% 15.417% 13 21.148 1747 1754 1767 rBV 2061146 4167923 100.00% 17.412% 14 23.287 1980 1987 1992 rBV 171898 334128 8.02% 1.396% 15 25.591 2231 2238 2248 rBV 1958973 4012971 96.28% 16.765%

16 33.642 3106 3115 3136 rBV2 1297246 3013232 72.30% 12.588% 17 37.874 3568 3576 3592 rBV2 718805 2121336 50.90% 8.862%

Sum of corrected areas: 23936835

8837.D GCMS0412.M Wed Apr 24 08:36:31 2002

NYC-WTC_000043703

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NYC-WTC_000043703Source: NYC Law Department, mirrored locally

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GCMS calibration table, May 2002 · Box DEP Box 25

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Laboratory document displaying a GCMS calibration table with retention times and response factors for deuterated standards from May 2002.

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