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← Document results/DEP Box 25/GCMS X 4/24/02 A 5/3/02
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GC/MS calibration table, sample AE08837, April 2002

Machine-extracted title · confidence 90%

Calibration data for GC/MS analysis of surrogate compounds including dichlorobenzenes and naphthalene from April 2002.

NYC-WTC_000043699–000043713

Folder label: “GCMS X 4/24/02 A 5/3/02”

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NYC 9/11 Public Portal Document yuantitatlon Report (V1 Reviewed;

Data File : C:\HPCHEM\1\DATA\APR2 302\8837.D Vial: 6 Acq On : 23 Apr 2002 7:18 pm Operator: Sample : gc/ms scan 4/15 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 24 8:14 2002 Quant Results File: GCMS0412.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Apr 17 11:48:30 2002 Response via : Initial Calibration DataAcq Meth : GCMS0412

Compound R.T. Qlon Response Cone Unit Qvalue 33) Hexachlorobenzene 0.00 284 0 N.D. 34) Phenanthrene 25.60 178 501 N.D. 35) Anthracene 25.60 178 501 N.D. 36) Di-n-butylphthalate 27.56 149 2893 N.D. 37) Fluoranthene 0.00 202 0 N.D. 40) Pyrene 0.00 202 0 N.D. 41) Butylbenzylphthalate 0.00 149 0 N.D. 42) Benzo(a)anthracene 33.64 228 3408 N.D. 43) Bis(2-ethylhexyl)phthalate 33.85 149 1476 N.D. 44) Chrysene 33.72 228 905 N.D. 46) Di-n-Octylphthalate 0.00 149 0 N.D. 47) Benzo(b)fluoranthene 36.70 252 537 N.D. 48) Benzo(k)fluoranthene 36.77 252 496 N.D. 4 9) Benzo(a)pyrene 37.88 252 2420 N.D. 50) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 51) Dibenz(a,h)anthracene 0.00 278 0 N.D. 52) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 8837.D GCMS0412.M Wed Apr 24 08:16:08 2002 Page 2

NYC-WTC_000043700

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NYC-WTC_000043700Source: NYC Law Department, mirrored locally

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GCMS calibration table, May 2002 · Box DEP Box 25

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Laboratory document displaying a GCMS calibration table with retention times and response factors for deuterated standards from May 2002.

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