Calibration data for GC/MS analysis of surrogate compounds including dichlorobenzenes and naphthalene from April 2002.
NYC-WTC_000043699–000043713Folder label: “GCMS X 4/24/02 A 5/3/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document UCIIU ICDUL — V 2 J. LVLW/
Data File : C:\HPCHEM\1\DATA\APR2302\8837.D Vial: 6 Acq On : 23 Apr 2002 7:18 pm Operator: Sample : gc/ms scan 4/15 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 24 8:14 2002 <Quant Results File: GCMS0412.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE tor)
xY* Title : 209 625/TCLP calibration table Last Update : Wed Apr 17 11:48:30 2002 Response via : Initial Calibration 1 DataAcq Meth : GCMS0412
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 12.22 152 538447 20.00 ug/1 -0.02 10) Naphthalene-d8 15.84 136 1949274 20.00 ug/1 -0.03 17) Acenaphthene-diO 21.15 164 1101025 20.00 ug/1 -0.02 30) Phenanthrene-diO 25.59 188 1610706 20.00 ug/1 -0.02 39) Chrysene-dl2 33.64 240 1037495 20.00 ug/1 -0.03 45) Perylene-dl2 37.87 264 631693 20.00 ug/1 -0.04
System Monitoring Compounds 2 8) TCMX 23.29 209 38173 6.92 ug/L -0.04 Spiked Amount 10.000 Recovery = 69.20% 38) 2,4-DDD 0.00 235 0 0.00 ug/mL Spiked Amount 5.000 Recovery = 0.00%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.51 74 197 N.D. 3) bis(2-Chloroethyl )ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2 -Dichlorobenzene 0.00 146 0 N.D. 7) 2,21 -oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.90 128 139 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 2 3) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.63 149 632 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 29) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. 31) N-Nitrosodiphenylamine 0.00 168 0 N.D. 32) 4-Bromophenyl-phenylether 0.00 248 0 N.D.
(#) = qualifier out of range (m) = manual integration 8837.D GCMS0412.M Wed Apr 24 08:16:07 2002 Page 1
NYC-WTC_000043699
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NYC-WTC_000043146
Laboratory document displaying a GCMS calibration table with retention times and response factors for deuterated standards from May 2002.
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GC/MS instrument calibration report for polycyclic aromatic hydrocarbons and chlorinated compounds using 40 µg/L standards, dated May 2-3, 2002.
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Calibration data sheet listing retention times and response factors for deuterated internal standards used in TCLP testing.
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Gas chromatography-mass spectrometry analysis of sample AE02785 performed on 3/11/2002, detecting 2,4-DDD and other unknown compounds.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052832
GC/MS analysis report for sample AE01043 showing surrogate recovery data generated on February 25, 2002.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000011817
Laboratory report documenting GCMS analysis of environmental sample AE04131 conducted on April 1, 2002.
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