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GCMS blank analysis report, May 6, 2002

Machine-extracted title · confidence 90%

Laboratory report documenting a GC/MS blank run to check for contamination in the analytical system on May 6, 2002.

NYC-WTC_000043547–000043559

Folder label: “GCMS X 3/26/02 No Analyses

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\1\DATA\MAY0602\LB.D Vial: 3 Acq On 6 May 2002 11:27 am Operator: Sample GC/MS SCAN 4/24 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.159 336 340 366 rBV 319629 719804 18.23% 3.542% 2 12.191 775 780 798 rBV 1248248 2809894 71.15% 13.827% 3 15.828 1171 1177 1194 rBV 1746052 3585127 90.79% 17.641% 4 21.134 1749 1756 1770 rBV 1937425 3949010 100.00% 19.432% 5 23.269 1984 1989 1996 rVB 166656 324934 8.23% 1.599%

6 25.579 2234 2241 2251 rBV2 1727466 3670083 92.94% 18.059% 7 26.486 2335 2340 2350 rBV 144041 275589 6.98% 1.356% 8 26.623 2350 2355 2368 rBV 42515 99331 2.52% 0.489% 9 28.080 2509 2514 2522 rBV 34048 65159 1.65% 0.321% 10 29.015 2612 2616 2626 rVB 25521 54596 1.38% 0.269%

11 33.633 3110 3120 3139 rBV2 1206103 2689282 68.10% 13.233% 12 33.853 3139 3144 3157 rVB 19468 55905 1.42% 0.275% 13 37.858 3573 3581 3601 rBV2 679952 2023752 51.25% 9.958%

Sum of corrected areas: 20322466

LB.D GCMS0501.M Wed May 08 11:53:41 2002

NYC-WTC_000043551

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NYC-WTC_000043551Source: NYC Law Department, mirrored locally

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