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GCMS calibration results for sample AE07311, April 2002

Machine-extracted title · confidence 100%

Laboratory report displaying GCMS calibration data for sample AE07311 conducted on April 3, 2002.

NYC-WTC_000046554–000046565

Folder label: “GCMS X 3/28/02 A 2/27/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\1\DATA\APR0302\LB.D Vial: 3 Acq On 3 Apr 2002 1:38 pm Operator: Sample gc/ms scan 3/28 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0403.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.228 342 347 355 rBV 23581 52336 1.55% 0.340% 2 12.249 779 785 801 rVB 980994 2320338 68.69% 15.081% 3 14.847 1063 1068 1074 rVB 128153 244514 7.24% 1.589% 4 15.563 1142 1146 1152 rBV 31313 65274 1.93% 0.424% 5 15.884 1175 1181 1194 rBV 1405942 2961969 87.68% 19.252%

6 21.190 1752 1759 1773 rBV 1605001 3378122 100.00% 21.956% 7 23.329 1983 1992 1999 rBV 117655 238415 7.06% 1.550% 8 25.634 2236 2243 2253 rBV 1436078 3110039 92.06% 20.214% 9 33.685 3108 3120 3139 rBV2 772096 1731347 51.25% 11.253% 10 33.905 3139 3144 3157 rVB 113904 239071 7.08% 1.554%

11 37.926 3575 3582 3599 rBV2 345730 1044194 30.91% 6.787%

Sum of corrected areas: 15385619

LB.D GCMS0403.M Tue Apr 09 13:09:19 2002

NYC-WTC_000046558

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NYC-WTC_000046558Source: NYC Law Department, mirrored locally

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