GCMS blank analysis results, sample AE04733, Apr 2002

NYC 9/11 Public Portal Document

LSC Area Percent Report

‘ Data File : C:\HPCHEM\l\DATA\MAR2802\LB.D Vial: 3 Acq On : 28 Mar 2002 10:29 am Operator: Sample : gc/ms scan 3/4 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 12.250 779 785 800 rVB 824615 1935638 69.61% 14.902% 2 15.885 1175 1181 1195 rBV 1196289 2467853 88.75% 19.000% 3 21.191 1753 1759 1767 rBV 1419358 2780761 100.00% 21.409% 4 25.635 2236 2243 2255 rBV 1296050 2601203 93.54% 20.026% 5 30.711 2791 2796 2803 rBV 162421 303293 10.91% 2.335%

6 33.695 3114 3121 3136 rVB2 653315 1511446 54.35% 11.636% 7 34.944 3252 3257 3262 rBV2 16329 38546 1.39% 0.297% 8 36.137 3381 3387 3397 rBV2 30995 90844 3.27% 0.699% 9 37.376 3516 3522 3531 rBV 33696 115216 4.14% 0.887% 10 37.936 3575 3583 3598 rBV 320469 939432 33.78% 7.233%

11 38.827 3672 3680 3690 rBV4 28392 128322 4.61% 0.988% 12 40.599 3863 3873 3880 rBV4 15804 76392 2.75% 0.588%

Sum of corrected areas: 12988946

LB.D GCMS0308.M Mon Apr 01 11:12:19 2002

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