GCMS calibration data for sample AE07108, April 2002

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Calibration table excerpt from GCMS analysis of sample AE07108 showing surrogate recovery data from April 19, 2002.

NYC-WTC_000043498–000043503

Folder label: “GCMS X 4/23/02 A 4/24/02”

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Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\APR1802\7108.D Vial: 27 Acq On : 19 Apr 2002 3:38 pm Operator: Sample : GC/MS SCAN 3/26 FB Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 22 8:292002 <Quant Results File: GCMS0419.RES

Quant Method C:\HPCHEM\1\METHODS\GCMS0419.M (RTE Integrator) ) Title 209 625/TCLP calibration table * kA Last Update Fri Apr 19 14:51:24 2002 " A Response via Initial Calibration p DataAcq Meth GCMS0412 e 0

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.22 152 674254 20.00 ug/1 -0.02 10) Naphthalene-d8 15.84 136 2468936 20.00 ug/1 -0.03 17) Acenaphthene-diO 21.15 164 1382141 20.00 ug/1 -0.02 30) Phenanthrene-diO 25.59 188 2030352 20.00 ug/1 -0.02 39) Chrysene-dl2 33.65 240 1348445 20.00 ug/1 -0.02 45) Perylene-dl2 37.88 264 896171 20.00 ug/1 -0.04

System Monitoring Compounds 28) TCMX 23.29 209 30671 2.66 ug/L -0.04 Spiked Amount 4.000 Recovery = 66.50% 38) 2,4-DDD 0.00 235 0 0.00 ug/mL Spiked Amount 5.000 Recovery = 0.00%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 . 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 0.00 128 0 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 21.53 165 256 N.D. 25) Diethylphthalate 22.63 149 733 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 29) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. 31) N-Nitrosodiphenylamine 0.00 168 0 N.D. 32) 4-Bromophenyl-phenylether 0.00 248 0 N.D.

(#) = qualifier out of range (m) = manual integration 7108.D GCMS0419.M Mon Apr 22 08:30:42 2002 Page 1

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