GCMS sample AE07107 analysis report with surrogate recovery, Apr 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\APRI8 02\7107.D Vial: 26 Acq On : 19 Apr 2002 2:40 pm Operator: Sample : GC/MS SCAN 3/26 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\GCMS0419.M (RTE Integrator) Title 209 625/TCLP calibration table Library C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.21 0.31 ug/1 56753 1,4-Dichlorobenzene-d4 12.21

Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 50 2 2 -Nonanqne, 9-hydroxy- 158 C9H1802 025368-56-3 33 3 Morpholine, 4-methyl- 101 C5H11NO 000109-02-4 9 4 1,8-Nonanediol, 8-methyl-________ 174 C10H22O2 054725-73-4 9 Abundance / Scan 344 (8.206 min): 7107.D (-) m/z 42.95 100.00% / 43

59 5000

101 7' I I 1l I I I I I I f I 171 i I I 1 I-

7.80 8.00 8.20 8.40 8.60 83 ............................. ‘ 1 i 1 ' ' 1 i 1 ' ' 1 i ‘ 1 1 1 11 1 I , 153 | ■ ■ ■ ■ i ■ ■ ■ ' i ■' ■ ■ ■ । ■ I । ■ ■ ■ ■ । m/z 59.05 54.70% m/z--> 10 20 30 40 50 60 70 80 90 100 110 Abundance #3245: 2-Pentanone, 4-hydroxy-4-methyl- 43

5000- 59 "nm ' 1 7.80 8.00 8.20 8.40 8.60 m/z 100.95 23.81% 31 83 101 1 I I I I — [ I " < 11, I I I I I' j I ri JI ....... 73 I I I I I I I I I I I 83 ....... I....... I I I I I I I I I I I I I I I

m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #11995: 2-Nonanone, 9-hydroxy- 43 58 _____________ VY___________ l i I । । । । । । । । r r । J । । ii । [ i-

7.80 8.00 8.20 8.40 8.60 5000 m/z 58.05 16.28%

71

m/z-> 1 ■ i 10 ‘ 1 1 1 i 1 20 - 30 40 TTT 50 _L 60 i 1 1 ■ ' i 70 1 1 80 82 h 90 100 110 Abundance #1640: Morpholine, 4-methyl- ........... A........... 43 7.80 8.00 8.20 8.40 8.60 m/z 41.05 8.92%

5000 101 15 71 27 56 i 1 1,1 1 1 ' 1'' I 11 11 I 1 i 1 1 i J n 1 1 1 ■ । • 1 1 * । 1 1 1 ' 1 1 1 1 1 । /w | i I I I | I I i I /AAAA j i I i i q I i I i । i ।

m/z-> 10 20 30 40 50 60 70 80 90 100 110 7.80 8.00 8.20 8.40 8.60

7107.D GCMS0419.M Mon Apr 22 08:34:15 2002 Page 1

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