GCMS analysis report, sample AE04417, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\MAR21O2\4418.D Vial: 9 Acq On : 21 Mar 2002 7:09 pm Operator: Sample : gc/ms scan 3/1 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

8.25 0.41 ug/1 64271 1,4-Dichlorobenzene-d4 12.27

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 36 2 2-Nonanone, 9-hydroxy- 158 C9H18O2 025368-56-3 28 3 Acetone 58 C3H60 000067-64-1 16 4 Ethanol, 1-methoxy-, acetate 118 C5H10O3 _ 004382-77-8 9 Abundance Scan 349 (8.247 min): 4418.D (-) m/z 43.. 00 100.00% i 43 59 5000 101 . t" ■ । r''11111 TTrTu । ■ । rTt" 83 8.00 8.20 8.40 8.60 -TTH 1 1491m— “' 1 ■''' I ‘ m/z 59.05 59.31% m/z-> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #64274: 2-Pentanone, 4-hydroxy-4-methyl- 43 MA_____ 5000 ■ i ■ ■ ■ ■ 1** ■ ■ i • ■ 59 8.00 8.20 8.40 8.60 m/z 101.0,5 27.89% 27 49 | 83 101 mmmm m/z-> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #11995: 2-Nonanone. 9-hydroxy 43 58 ...................... ...................... 8.00 8.20 8.40 8.60 5000 m/z 58.0.5 23.54% 71 82 TIWWTIPWTWTTPTTITITWIWWW)WWWIWTTRTTT m/z—> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #62322: Acetone 43 8.00 8.20 8.40 8.60 m/z 42.15 9.84% 5000 58 27 FTmpasgrT Tp^TTYrrrrpTTTTTTTTp-rTTjTTTTpTT-ri-rTT^^ miz—> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 8.00 8.20 8.40 8.60

4418.D GCMS0308.M Fri Mar 22 09:40:19 2002 Page 2

NYC-WTC_000012336