GCMS analysis results for sample AE06996, April 2002

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Data File C:\HPCHEM\l\DATA\APR0405\6996.D Vial: 25 Acq On 6 Apr 2002 8:33 pm Operator: Sample gc/ms scan 3/26 Inst : GC/MS 209 Mise Multiplr: 2.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0408.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.76 40.00 ug/1 411654000 1,4-Dichlorobenzene-d4 12.26

Hit# of 5 ^Tentative ID MW MolForm CAS# Qual

1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 53 2 2-Nonanone, 9-hydroxy- 158 C9H1802 025368-56-3 25 3 Propane/ 2-ethoxy-2-methyl - 102 C6H140 000637-92-3 17 4 2-Propanol, 2 - methyl-____ 74 C4H10O 000075-65-0 12 Abundance Scan 404 (8.758 min): 6996.D (-) m/ z 43.00 100.00% 43 59 5000 101 8.40 8.60 8.80 9.00 9.20

m/z-> 0- । ■ । 1 • ■ ■ i ■ ■ ■ ■ । ■ - 37 10 20 30 +5053+ —60 6970TOTTTTT II ■ < | ' 40 77 83 80 90 94 , 100 1 i 110 117 1 1 i 1 1 120 m/z 59.05 66.42% Abundance #64275: 2-Pentanone, 4-hydroxy-4-methyl- 43

5000 I I । i । I[ i । । TI j i । । । । । । i [ T 59 8.40 8.60 8.80 9.00 9.20 m/ z 10 0.95 28.09% 15 31 101 -------------HI 83 | T——t ' I ' ‘ ' I ■ ■ ■ ■ I ■' ■ 1 ■ I ■ • ' l ; ■ ■ - ■ l ■ 1 ■ ■ l 1 ■ Mz-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #11995: 2-Nonanone, 9-hydroxy- 43 58

8.40 8.60 8.80 9.00 9.20 5000 m/z 58.00 20.44%

82 71 — - +.. 1 ■ ‘ 11m 1 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #63580: Propane, 2-ethoxy-2-methyl- ....... \ 59 8.40 8.60 8.80 9.00 9.20 m/z 41.05 10.59% 5000 87 41 31 _.... . ....... il ' ' I ' ' । । । । ■ । TI I I I I I 1 1 I I [ 1 I TI I I I I I I I I F I I 1 1 I I ] I T 1 I LIT T I I It l 1 1 I 1 ' ' ' I 1 ' 1 1 I 1 ' ' 1 IT I I I I I m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 8.40 8.60 8.80 9.00 9.20

6996.D GCMS0408.M Mon Apr 15 14:44:41 2002 Page 1

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