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GCMS analysis report for sample AE09453, May 2002

Machine-extracted title · confidence 100%

GCMS results for sample AE09453 showing surrogate recovery and unknown compounds dated May 6, 2002.

NYC-WTC_000043282–000043290

Folder label: “GCMS X 4/22/02 A 5/3/02

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Scanned page image, NYC-WTC_000043287
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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\1\DATA\MAY0202\9453.D Vial: 18 Acq On 3 May 2002 7:38 am Operator: Sample GC/MS SCAN 4/22 FB Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.162 337 341 359 rBV 359230 791381 24.11% 4.834% 2 12.194 776 781 799 rVB 1045420 2356435 71.79% 14.393% 3 15.832 1171 1178 1191 rBV 1437674 2965557 90.34% 18.114% 4 21.138 1750 1757 1774 rBV 1567064 3282608 100.00% 20.050% 5 23.273 1983 1990 1996 rVB 175769 340784 10.38% 2.082%

6 25.582 2235 2242 2253 rBV2 1422373 2988943 91.05% 18.257% 7 33.637 3115 3121 3133 rBV2 908304 2067079 62.97% 12.626% 8 37.870 3575 3583 3596 rBV2 547059 1579049 48.10% 9.645%

Sum of corrected areas: 16371836

9453 .D GCMS0501.M Fri May 03 12:23:36 2002

NYC-WTC_000043287

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NYC-WTC_000043287Source: NYC Law Department, mirrored locally

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