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GCMS analysis report for sample AE09452, May 2002

Machine-extracted title · confidence 100%

GCMS results for sample AE09452 showing surrogate recovery and unknown compounds dated May 6, 2002.

NYC-WTC_000043273–000043281

Folder label: “GCMS X 4/22/02 A 5/3/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\1\DATA\MAY0202\9452 .D Vial: 17 Acq On 3 May 2002 6:38 am Operator: Sample GC/MS SCAN 4/22 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.161 337 341 347 rBV 454145 882668 24.12% 4.986% 2 12.193 776 781 794 rVB 1202307 2620891 71.63% 14.804% 3 15.831 1171 1178 1190 rBV 1609591 3312643 90.53% 18.711% 4 21.137 1750 1757 1775 rBV 1762230 3659069 100.00% 20.667% 5 23.272 1982 1990 1997 rBV 194341 402264 10.99% 2.272%

6 25.581 2235 2242 2252 rBV2 1528943 3275862 89.53% 18.503% 7 33.636 3115 3121 3135 rBV2 896102 2062886 56.38% 11.652% 8 37.870 3575 3583 3598 rBV2 515601 1488202 40.67% 8.406%

Sum of corrected areas: 17704485

9452.D GCMS0501.M Fri May 03 12:23:27 2002

NYC-WTC_000043278

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NYC-WTC_000043278Source: NYC Law Department, mirrored locally

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