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← Document results/DEP Box 25/GCMS X 4/18/02 A 5/1/02
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GCMS analysis results, sample AE09393, May 8, 2002

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Laboratory report for DEP Box 25 showing GCMS analysis of sample AE09393 with unknown compounds and surrogate data from May 8, 2002.

NYC-WTC_000043079–000043096

Folder label: “GCMS X 4/18/02 A 5/1/02

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NYC 9/11 Public Portal Document

Data File C:\HPCHEM\l\DATA\MAY0102\9393.D Vial: 11 Acq On 1 May 2002 5:16 pm Operator: Sample gc/ms scan 4/18 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 2 11:47 2002 Quant Results File: GCMS0501.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed May 01 10:40:31 2002 Response via : Initial Calibration DataAcq Meth : GCMS0501

Compound R.T. Qlon Response Cone Unit Qvalue 35) Anthracene 25.59 178 291 N.D. 36) Di-n-butylphthalate 27.55 149 3276 N.D. 37) Fluoranthene 0.00 202 0 N.D. 3 9) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo(a)anthracene 33.64 228 2392 N.D. 42) Bis(2-ethylhexyl)phthalate 33.86 149 17124 0.75 ug/1 99 43) Chrysene 33.64 228 2391 N.D. 45) Di-n-Octylphthalate 35.61 149 434 N.D. 46) Benzo(b)fluoranthene 0.00 252 0 N.D. 47) Benzo(k)fluoranthene 0.00 252 0 N.D. 48) Benzo(a)pyrene 37.87 252 2291 N.D. 49) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 9393 .D GCMS0501,M Thu May 02 11:48:13 2002 Page 2

NYC-WTC_000043082

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NYC-WTC_000043082Source: NYC Law Department, mirrored locally

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GCMS calibration table, May 2002 · Box DEP Box 25

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Laboratory document displaying a GCMS calibration table with retention times and response factors for deuterated standards from May 2002.

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