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ICPMS daily performance check report, April 23, 2002

Machine-extracted title · confidence 95%

Daily instrument performance verification log for ICPMS analysis including intensity and standard deviation data for multiple elements.

NYC-WTC_000040976–000041063

Folder label: “ICPMS 4/23/02”

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: AE08260 Sample Date/Time: Tuesday, April 23, 2002 11:29:20 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: d:\elandata\Method\NYC.mth Dataset File: d:\elandata\Dataset\new york city\AE08260.678 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Cone. Mean Cone. RSD Sample Unit Be 9 8.667 43.684 -0.000 -0.00231 435.61 ug/L > Se-1 45 488504.069 1.464 488504.069 ug/L Cr 52 9900.156 2.421 0.005 0.24786 4.73 ug/L Cr 53 1439.128 1.235 0.001 0.63690 5.64 ug/L Mn 55 242246.486 1.724 0.494 17.44503 1.04 ug/L Ni 60 889.386 4.981 0.001 0.30468 7.33 ug/L Cu 63 5841.602 1.744 0.011 1.07373 0.98 ug/L Cu 65 2869.815 0.824 0.005 1.04805 1.76 ug/L Zn 66 18897.153 2.810 0.191 11.46290 2.37 ug/L Zn 67 3102.561 3.246 0.031 10.14491 3.57 ug/L Zn 68 14302.386 1.475 0.144 11.59042 1.21 ug/L > Ge 72 94854.574 0.536 94854.574 ug/L As 75 987.556 9.136 0.010 0.50138 9.09 ug/L Se 77 197.006 6.315 0.001 0.48289 15.14 ug/L Se 82 188.337 4.818 0.001 0.38153 10.33 ug/L Ag 107 86.668 12.338 -0.000 -0.05570 1.99 ug/L Cd 111 850.761 2.919 -0.000 -0.06677 7.56 ug/L Cd 114 140.713 14.106 -0.000 -0.00116 322.15 ug/L > In 115 1253310.363 1.507 1253310.363 ug/L Sb 121 425.014 3.561 0.000 0.04442 5.12 ug/L Sb 123 321.664 2.035 0.000 0.04295 2.91 ug/L Ba 135 40642.725 0.890 0.023 16.03878 1.87 ug/L Ba 137 71040.599 1.899 0.041 16.00961 1.67 ug/L > Tb 159 1727197.984 1.519 1727197.984 ug/L Ho 165 1708460.634 1.416 -0.003 ug/L Hg 201 33.334 22.113 -0.000 -0.01933 35.90 ug/L Hg 202 74.668 11.391 -0.000 -0.02295 15.74 ug/L TI 205 728.036 4.640 0.000 0.00290 65.58 ug/L Pb 208 2886.876 1.881 0.001 0.03363 7.74 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery Int Std % Recovery Spike % Recovery Dilution % Diff Dup. Rei. % Diff ’ Be 9 > Sc-1 45 105.200 Cr 52

Sample ID: AE08260 Report Date/Time: Tuesday, April 23, 200211:31:56 Page 1

NYC-WTC_000041052

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NYC-WTC_000041052Source: NYC Law Department, mirrored locally

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