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ICPMS daily performance check report, April 11, 2002

Machine-extracted title · confidence 95%

Daily instrument performance verification log for ICPMS analysis including intensity and standard deviation data for multiple elements.

NYC-WTC_000040598–000040646

Folder label: “ICPMS 4/11/02

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: AE06987 Sample Date/Time: Thursday, April 11, 2002 14:31:44 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: d:\elandata\Method\NYC.mth Dataset File: d:\elandata\Dataset\new york city\AE06987.484 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Cone. Mean Cone. RSD Sample Unit Be 9 6.667 8.660 -0.000 -0.01608 8.49 ug/L > Se-1 45 451703.957 1.148 451703.957 ug/L Cr 52 13059.178 3.627 0.014 0.75233 10.12 ug/L Cr 53 2859.478 2.086 0.005 2.39685 1.53 ug/L Mn 55 647273.785 1.207 1.429 47.79884 1.48 ug/L Ni 60 2395.673 2.529 0.005 1.18797 1.98 ug/L Cu 63 6611.803 0.687 0.014 1.34711 0.62 ug/L Cu 65 3149.577 2.773 0.007 1.33611 4.06 ug/L Zn 66 9750.660 2.708 0.104 5.93860 2.86 ug/L Zn 67 1906.886 0.397 0.020 6.62981 2.41 ug/L Zn 68 8187.102 2.523 0.088 7.15180 3.24 ug/L > Ge 72 87160.812 1.930 87160.812 ug/L As 75 577.631 38.276 0.006 0.31632 39.29 ug/L Se 77 316.675 10.269 0.003 1.52057 13.13 ug/L Se 82 136.669 1.841 0.001 0.23277 10.63 ug/L Ag 107 114.669 13.548 -0.001 -0.13947 1.16 ug/L Cd 111 779.294 3.922 -0.000 -0.05742 30.80 ug/L Cd 114 90.459 4.531 0.000 0.00485 14.34 ug/L > In 115 1184745.478 1.784 1184745.478 ug/L Sb 121 567.023 4.582 0.000 0.06008 6.90 ug/L Sb 123 466.866 5.298 0.000 0.06643 6.19 ug/L Ba 135 71816.345 2.044 0.043 29.78259 2.01 ug/L Ba 137 129149.032 2.935 0.077 31.09397 2.52 ug/L > Tb 159 1677962.537 0.612 1677962.537 ug/L Ho 165 1744220.077 1.287 0.079 ug/L TI 205 629.028 8.217 -0.000 -0.03502 6.88 ug/L Pb 208 7810.039 1.660 0.004 0.20130 1.50 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery Int Std % Recovery Spike % Recovery Dilution % Diff Dup. Rei. % Diff ' Be 9 > Sc-1 45 95.207 Cr 52 Cr 53 Mn 55

Sample ID: AE06987 Report Date/Time: Thursday, April 11,2002 14:33:31 Page 1

NYC-WTC_000040639

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NYC-WTC_000040639Source: NYC Law Department, mirrored locally

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