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ICPMS daily performance check report, April 23, 2002

Machine-extracted title · confidence 95%

Daily instrument performance verification log for ICPMS analysis including intensity and standard deviation data for multiple elements.

NYC-WTC_000040976–000041063

Folder label: “ICPMS 4/23/02”

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: AE08935 Sample Date/Time: Tuesday, April 23, 2002 10:48:11 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: d:\elandata\Method\NYC.mth Dataset File: d:\elandata\Dataset\new york city\AE08935.673 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Cone. Mean Cone. RSD Sample Unit Be 9 6.333 9.116 -0.000 -0.00821 16.00 ug/L > Se-1 45 476164.730 2.290 476164.730 ug/L Cr 52 11457.331 1.457 0.008 0.45678 10.74 ug/L Cr 53 1839.205 2.967 0.002 1.05929 1.35 ug/L Mn 55 321382.733 1.141 0.673 23.77470 1.38 ug/L Ni 60 1250.432 1.423. 0.002 0.48379 4.34 ug/L Cu 63 77399.877 0.736 0.162 15.78279 1.97 ug/L Cu 65 38612.888 1.135 0.081 15.76304 2.00 ug/L Zn 66 23330.467 1.029 0.245 14.71461 0.74 ug/L Zn 67 3764.817 1.708 0.039 12.82937 1.07 ug/L Zn 68 17581.832 1.968 0.184 14.81434 1.98 ug/L Ge 72 92110.290 1.706 92110.290 ug/L As 75 918.891 7.516 0.009 0.47913 6.80 ug/L Se 77 219.429 12.056 0.001 0.65345 22.22 ug/L Se 82 182.337 6.612 0.001 0.37841 12.04 ug/L Ag 107 154.336 0.374 -0.000 -0.04827 0.41 ug/L Cd 111 880.345 1.465 -0.000 -0.04795 22.36 ug/L Cd 114 133.793 6.772 -0.000 -0.00193 92.08 ug/L > In 115 1229882.834 1.552 1229882.834 ug/L Sb 121 600.359 2.506 0.000 0.06635 4.30 ug/L Sb 123 462.253 1.644 0.000 0.06559 3.45 ug/L Ba 135 47517.017 1.470 0.028 18.87154 1.47 ug/L Ba 137 81817.413 1.735 0.048 18.55885 2.33 ug/L Tb 159 1716505.372 1.028 1716505.372 ug/L Ho 165 1692778.158 0.367 -0.006 ug/L Hg 201 39.334 12.541 -0.000 -0.01361 35.10 ug/L Hg 202 84.001 9.449 -0.000 -0.01909 16.26 ug/L TI 205 765.707 9.516 0.000 0.00469 61.14 ug/L Pb 208 454009.973 0.238 0.263 14.64669 0.93 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery Int Std % Recovery Spike % Recovery Dilution % Diff Dup. Rei. % Diff ’ Be 9 > Sc-1 45 102.542 Cr 52

Sample ID: AE08935 Report Date/Time: Tuesday, April 23,2002 10:50:04 Page 1

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NYC-WTC_000041037Source: NYC Law Department, mirrored locally

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