GCMS surrogate recovery data for sample AE07638, April 2002

NYC 9/11 Public Portal Document LSC Area Percent Report

Data File : C:\MSDCHEM\1\DATA\020410\07638.D Vial: 10 Acq On : 10 Apr 2002 6:51 pm Operator: Nefliu Sample : field bik Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Method : C:\MSDCHEM\1\METHODS\SCANAPR0902.M (Chemstation Integrator) Title : Method 508 GC/MS Scan

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.273 13 33 45 BV 6 3148 139098 0.71% 0.146% 2 3.349 45 46 55 W 3 2187 64573 0.33% 0.068% 3 3.420 55 58 61 W 3 1193 15542 0.08% 0.016% 4 10.659 1280 1290 1310 W 474680 12985792 66.38% 13.674% 5 14.689 1968 1976 1991 W 4 7025 183651 0.94% 0.193%

6 15.770 2147 2160 2180 W 687495 17075374 87.28% 17.981% 7 23.655 3488 3502 3514 PV 748869 19339515 98.86% 20.365% 8 26.722 4009 4024 4034 W 3 51845 1128685 5.77% 1.189% 9 30.277 4620 4629 4637 W 2 1654 56890 0.29% 0.060% 10 30.894 4717 4734 4749 PV 2 699291 19563140 100.00% 20.601%

11 31.123 4769 4773 4783 W 2 1814 56931 0.29% 0.060% 12 33.973 5254 5258 5266 W 2 1721 38842 0.20% 0.041% 13 39.091 6119 6129 6152 PV 2 864470 15741445 80.46% 16.576% 14 39.232 6152 6153 6155 W 1107 7376 0.04% 0.008% 15 42.299 6665 6675 6700 PV 448383 8546754 43.69% 9.000%

16 42.457 6700 6702 6709 W 3 1213 20166 0.10% 0.021%

Sum of corrected areas: 94963774

07638.D SCANAPR0902,M Fri Apr 12 14:37:13 2002 Page 1

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