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GCMS surrogate recovery data for sample AE07765, April 2002

Machine-extracted title · confidence 100%

Record of surrogate compound recovery rates for sample AE07765 analyzed on April 18, 2002.

NYC-WTC_000040279–000040285

Folder label: “GCMS X 4/3/02 A 4/10/02

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NYC 9/11 Public Portal Document LSC Area Percent Report

Data File : C:\MSDCHEM\1\DATA\020410\05286.D Vial: 12 Acq On : 10 Apr 2002 8:43 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Method : C:\MSDCHEM\1\METHODS\SCANAPR0902.M (Chemstation Integrator) Title : Method 508 GC/MS Scan

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.285 22 35 37 PV 4 2764 91517 0.42% 0.086% 2 3.302 37 38 46 W 3 2108 51465 0.23% 0.048% 3 3.355 46 47 50 W 2 1004 12351 0.06% 0.012% 4 3.385 50 52 54 W 1020 8520 0.04% 0.008% 5 10.659 1279 1290 1311 W 542047 14333642 65.36% 13.392%

6 14.683 1959 1975 1986 PV 2 17076 424019 1.93% 0.396% 7 15.770 2145 2160 2170 BV 758756 18777570 85.62% 17.545% 8 16.005 2186 2200 2203 PV 1597 30015 0.14% 0.028% 9 23.655 3489 3502 3514 W 845875 21509843 98.08% 20.097% 10 26.722 4016 4024 4037 W 3 60617 1344425 6.13% 1.256%

11 30.265 4621 4627 4635 PV 2188 58278 0.27% 0.054% 12 30.894 4718 4734 4747 PV 2 791851 21931783 100.00% 20.492% 13 31.141 4760 4776 4781 PV 2 2544 77846 0.35% 0.073% 14 33.979 5250 5259 5272 W 12237 276697 1.26% 0.259% 15 39.096 6121 6130 6151 PV 2 948733 17981593 81.99% 16.801%

16 39.226 6151 6152 6165 VB 1733 45755 0.21% 0.043% 17 42.299 6659 6675 6703 PV 547038 10072764 45.93% 9.411%

Sum of corrected areas: 107028083

05286.D SCANAPR0902 ,M Thu Apr 11 14:08:25 2002 Page 1

NYC-WTC_000040281

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NYC-WTC_000040281Source: NYC Law Department, mirrored locally

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