GCMS surrogate recovery data for sample AE07633, April 2002

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\MSDCHEM\1\DATA\020410\07633.D Vial: 13 Acq On 10 Apr 2002 9:39 pm Operator: Nefliu Sample sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Method : C:\MSDCHEM\1\METHODS\SCANAPR0902.M (Chemstation Integrator) Title : Method 508 GC/MS Scan

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.285 21 35 37 PV 3 4650 153148 0.75% 0.153% 2 3.308 37 39 40 W 2 4576 56336 0.28% 0.056% 3 3.326 40 42 67 W 3 4492 308652 1.52% 0.308% 4 4.548 242 250 255 W 3 3428 58060 0.29% 0.058% 5 5.042 324 334 337 PV 2 1634 22757 0.11% 0.023%

6 10.659 1268 1290 1313 W 482607 13416124 65.91% 13.406% 7 14.689 1959 1976 1985 PV 26142 620809 3.05% 0.620% 8 15.770 2147 2160 2176 PV 712089 17637601 86.65% 17.624% 9 23.655 3490 3502 3516 PV 773130 20085908 98.67% 20.071% 10 26.722 4014 4024 4041 W 2 63582 1416694 6.96% 1.416%

11 30.260 4621 4626 4630 PV 2 1848 39626 0.19% 0.040% 12 30.894 4720 4734 4754 W 2 728896 20356009 100.00% 20.340% 13 31.147 4761 4777 4782 W 2 2066 71448 0.35% 0.071% 14 33.979 5248 5259 5266 W 2 3433 93158 0.46% 0.093% 15 39.091 6118 6129 6163 PV 2 890143 16547905 81.29% 16.535%

16 42.299 6667 6675 6700 PV 476108 9192209 45.16% 9.185%

Sum of corrected areas: 100076446

07633.D SCANAPR0902.M Fri Apr 12 14:27:37 2002 Page 1

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