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GCMS surrogate recovery data for sample AE07634, April 2002

Machine-extracted title · confidence 100%

Record of surrogate compound recovery rates for sample AE07633 analyzed on April 18, 2002.

NYC-WTC_000040203–000040211

Folder label: “GCMS X 4/3/02 A 4/10/02

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Scanned page image, NYC-WTC_000040209
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document Library Search Compound Report

4 Data File : C:\MSDCHEM\1\DATA\020410\07634.D Vial: 9 Acq On : 10 Apr 2002 5:55 pm Operator: Nefliu Sample : field blk Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\l..-\SC7kNAPR0902.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 1 2-Butyne-1,4-diol Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 3.29 0.20 ug/1 135575 1,4-Dichlorobenzene-d4 10.66 Hit# of 5 Tentative ID MW MolForm CAS# Qual

l 2-Butyne-l,4-diol 86 C4H602 000110-65-6 3 2 Imidazol, 4-fluoro- 86 C3H3FN2 030086-17-0 2 3 Ethyl Chloride 64 C2H5C1 000075-00-3 1 4 2-Methyl-3-vinyl-oxirane 84 C5H80 006790-37-0 1 Abundance Scan 36 (3.291 min): 07634.D (-20) (-) m/z 49.00 100.00% 49 84

5000

40 3.20 3.30 3.40 3.50 3.60 3.70 O+ " r " ' i " " r " 1111111" " I" " 11" 111’ I" " I " " I " " I " 111" '' I ’IITT"T[T jn/z^84^ ■n/z—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #108388: 2-Butyne-1,4-dioI 29 39 57

5000 68 3.20 3.30 3.40 3.50 3.60 3.70 26 43 51 m/z 86.00 58.85% MW m/z-> ‘11" " i " " i1 5 —l33s 14754 460,.65. 717477 81 85 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 ' i111 ri'"111 "f11"1111"i1 w/MMut Abundance #34862: Imidazol, 4-fluoro- 85

3.20 3.30 3.40 3.50 3.60 3.70 5000 m/z47.0051.32%

59 A /Mhalv, A k AW Of '1 r ''11" '11' " ' I ■ ‘1111 ■1' i1111111111111111111111111111 i I " ' ‘ 1111' 111'11111' I T m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #107943: Ethyl Chloride '111’’’1’—11111EIT0I1T1UT I’’ 28 3.20 3.30 3.40 3.50 3.60 3.70 m/z 51.05 31.57% 5000

25 35 49 64 .M 0 1215 TITH TIHTT 31..438. H TTH 60 . 67.............. m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 ■ ■ ।1' ■1111111 ■ ■'' ।111111"11'1 3.20 3.30 3.40 3.50 3.60 3.70

07634.D SCANAPR0902.M Tue Apr 30 13:40:32 2002 Page 3

NYC-WTC_000040209

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NYC-WTC_000040209Source: NYC Law Department, mirrored locally

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