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Document / 2 pages

GCMS batch record header for Method 508, April 2002

Machine-extracted title · confidence 90%

Fragmented document header from DEP Box 23 regarding GCMS analysis of World Trade Center samples.

NYC-WTC_000040046–000040047

Folder label: “GCMS X 3/26/02 A 4/6/02

Page image
Scanned page image, NYC-WTC_000040047
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

* v DFTPP % Data File C:\HPCHEM\1\DATA\APR0405\DFTPP1.D Vial: 1 Acq On 6 Apr 2002 5:45 am Operator: Sample Inst : GC/MS 2 09 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table

Abundance TIC: DFTPP1.D 2000000

1500000

1000000

500000

JI 0-1 ' 1 1 | ' 1 ' T' 1 1V*T1 1 7 1 p' 1 1 1 | 1 1 1 1 | 1 1 ' ‘ I 1 1 1 1 I 1 1 1 1 I 1 1 1 Ti ___ ______________________ —I i i । r i i i j j i i i । i < « J j i i i । j i । । i | । i >> J I । > । | > i J । ] । । । » | Time-> 25.00 25.20 25.40 25.60 25.80 26.00 26.20 26.40 26.60 26.80 27.00 27.20 27.40 27.60 27.80 28.00 28.20 28.40 28.60 Abundance Scan 2372 (26.818 min): DFTPP1.D (-) 198 250000

200000 442

150000 69 127 255 100000 51 110 275 50000 224 93 0 37 ++ 111 ■1 1 141H r f r। r ‘ 1 + 167 18114 411242. 26323346 365 383 403 423_ Hrr r I 1 I I I 1 11 tft—I I II I II I IIITTT I I I I I I I I I TI 1‘/tI

m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 440

Spectrum Information: Scan 2372

Target Rei. to Lower Upper Rei. Raw Result Mass Mass Limit% Limit% Abn% Abn Pass/Fail

51 198 30 60 34.8 91757 PASS 68 69 0.00 2 0.0 0 PASS 69 198 0.00 100 46.3 121963 PASS 70 69 0.00 2 0.0 0 PASS 127 198 40 60 43.5 114766 PASS 197 198 0.00 1 0.0 0 PASS 198 198 100 100 100.0 263542 PASS 199 198 5 9 6.7 17776 PASS 275 198 10 30 23.3 61387 PASS 365 198 1 100 2.5 6666 PASS 441 443 0.01 100 96.6 35632 PASS 442 198 40 110 72.5 191134 PASS 443 442 17 23 19.3 36880 PASS

DFTPP1.D GCMS0412.M Mon Apr 15 13:18:02 2002

NYC-WTC_000040047

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NYC-WTC_000040047Source: NYC Law Department, mirrored locally

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