GCMS analysis results for sample AE06585, April 15, 2002

NYC 9/11 Public Portal Document

.* Quantitation Report (QT Reviewed)

4" Data File : C:\MSDCHEM\l\DATA\041502\C25A0415.D Vial: 2 Acq On : 15 Apr 2002 10:47 am Operator: Bohik Sample : C25 Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: BENZO.P Quant Time: Apr 15 15:08:47 2002 Quant Results File: 5080402BBC.RES

Quant Method : C:\MSDCHEM\1\5973N\5080402BBC.M (RTE Integrator) Title : Quantitation For Method 508gcscan Last Update : Mon Apr 15 14:48:10 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 9.41 152 400350 40.00 ug/L 0.00 10) Naphthalene-d8 12.89 136 1636784 40.00 ug/L 0.00 17) Acenaphthene-dlO 17.99 164 903638 40.00 ug/L 0.00 30) Phenanthrene-diO 22.34 18 8 1286032 40.00 ug/L 0.00 39) Chrysene-dl2 30.15 24 G 1009401 40.00 ug/L 0.00 45) Perylene-dl2

J1 34.01 264 635733 40.00 ug/L 0.00

System Monitoring Compounds 2 8) TCMX (SURR) 19.95 244 35182 9.76 ug/L 0.00

o‘w;¥ Spiked Amount 5.000 Recovery = 195.20% 38) 2,4-DDD (SURR) 0.00 235 0 0.00 ug/L ) Spiked Amount 5.000 Recovery = 0.00%

Target Compounds Qvalue l 2) N-nitroso-dimethyl amine 3.43 74 512507m 44.27 ug/L 3) bis(2-chloroethyl) ether 8.85 93 859159 50.61 ug/L 80 4) 1,3 - Dichlorobenze 9.24 146 725538 52.31 ug/L 96 5) 1,4 - Dichlorobenzene 9.45 146 772807 52.05 ug/L 99 6) 1,2 - Dichlorobenzene 7) 2,2 ' - oxybis (l-Chloropr 8) N-Nitroso-di-n-propylamine 9.32 10.3 0 10.63 146 45 70 630086 1300341 617541 51.92 ug/L 51.35 ug/L 51.04 ug/L 99 93 98 U0H 0 9) Hexachloroethane 10.72 117 348946 52.85 ug/L 95 11) Nitrobenzene 10.97 77 831117 52.32 ug/L 98 12) Isophorone 11.68 82 1648501 52.17 ug/L 98 13) bis(2-Chloroethoxy) methan 12.43 93 1003546 52.06 ug/L 98 14) 1,2,4-Trichlorobenzene 12.77 180 566727 53.52 ug/L 100 15) Naphthalene 12.94 128 2106183 52.62 ug/L 99 16) Hexachlorobutadiene 13.40 225 272958 53.48 ug/L 95 18) Hexachlorocyclopentadiene 15.46 237 210132 49.69 ug/L 99 19) 2-chloronaphthalene 16.36 162 1000820 54.75 ug/L 98 20) Dimethylphthalate 17.46 163 1331517 51.23 ug/L 99 21) 2,6-Dinitrotoluene 17.57 165 256053 50.58 ug/L 93 22) Acenaphthylene 17.55 152 1774478 53.10 ug/L 99 2 3) Acenaphthene IS . 08 153 1100347 52.05 ug/L 99 24) 2,4-Dinitrotoluene 18.72 165 277021 45.43 ug/L 95 25) Diethylphthalate 19.59 149 1159006 53.71 ug/L 99 26) 4-Chlorophenyl-phenyl ethe 19.75 204 628951 52.72 ug/L 99 27) Fluorene 19.61 166 1323974 54.29 ug/L 99 29) Azobenzen/ 1,2-Diphenylhyd 20.20 77 1912987 50.98 ug/L 95 31) N-Nitrosodiphenylamine 20.12 169 754011 54.99 ug/L 98 32) 4-Bromophenyl-phenyl ether 21.18 248 309695 52.04 ug/L 91 33) Hexachlorobenzene 21.20 284 280006 50.34 ug/L 89 34) Phenanthrene 22.41 178 1865246 52.34 ug/L 100 35) Anthracene 22.56 178 1881980 51.77 ug/L 99 36) Di-n-butylphthalate 24.51 149 2197178 53.91 ug/L 99 37) Fluoranthene 25.91 202 1983846 52.49 ug/L 88 4 0) Pyrene 26.53 202 1963924 51.59 ug/L 90 41) Butylbenzylphthalate 28.90 149 932398 53.02 ug/L 91 42) Benzo (a) antracene 30.13 228 1559574 50.73 ug/L 98 43) Bis (2-ethylhexyl) phthala 3 0.77 149 1341903 53.73 ug/L 97 44) Chrysene 30.22 228 1575870 51.79 ug/L 99

(#) = qualifier out of range (m) = manual integration C25A0415.D 50S0402BBC.M Mon Apr 15 15:09:16 2002 Page 1

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