GCMS quantitative results for sample AE07173, April 24, 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

, Data File : C:\MSDCHEM\l\DATA\041802\REFA0418.D Vial: 6 Acq On : 18 Apr 2002 12:47 pm Operator: Bohlk Sample : REFl 3/27/02 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: BENZO.P Quant Time: Apr 24 08:19:08 2002 Quant Results File: 5080402BBC.RES

Quant Method : C:\MSDCHEM\l\5973N\5080402BBC.M (RTE Integrator) Title : Quantitation For Method 508gcscan Last Update : Wed Apr 24 08:08:47 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 9.41 152 557474 40.00 ug/L 0.00 10) Naphthalene-d8 12.89 136 2376819 40.00 ug/L 0.00 17) Acenaphthene-dlO 17.99 164 1309776 40.00 ug/L 0.00 30) Phenanthrene-dlO 22.35 188 1876194 40.00 ug/L 0.00 39) Chrysene-dl2 . 30.15 240 1484496 40.00 ug/L 0.00 45) Perylene-dl2 34.02 264 917607 40.00 ug/L 0.00

System Monitoring Compounds 28) TCMX (SURR) 19.95 244 28351 5.42 ug/L 0.00 Spilled Amount 4.000 Recovery = 135.50% 38) 2,4-DDD (StJRR) 0.00 235 0 0.00 ug/L Spiked Amount 10.000 Recovery = 0.00%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 3.50 74 135553m 8.41 ug/L 3) bis(2-chloroethyl) ether 8.85 93 308495 13.05 ug/L 80 4) 1,3 - Dichlorobenze 9.24 146 268829 13.92 ug/L 99 5) 1,4 - Dichlorobenzene 9.45 146 269002 13.01 ug/L 96 6) 1,2 - Dichlorobenzene 9.83 146 239400 14.17 ug/L 99 7) 2,2 ' - oxybis (1-Chloropr 10.30 45 567465 16.09 ug/L 91 8) N-Nitroso-di-n-propylamine 10.62 70 240531 14.28 ug/L 94 9) Hexachloroethane 10.72 117 113897 12.39 ug/L 99 11) Nitrobenzene 10.97 77 273490 11.86 ug/L 96 12) Isophorone 11.68 82 630158 13.73 ug/L 97 13) bis(2-Chloroethoxy) methan 12.43 93 359212 12.83 ug/L 96 14) 1,2,4-Trichlorobenzene 12.76 180 214090 13.92 ug/L 97 15) Naphthalene 12.94 128 925570 15.92 ug/L 98 16) Hexachlorobutadiene 13.39 225 110999 14.98 ug/L 95 18) Hexachlorocyclopentadiene 15.47 237 23716 3.87,ug/L 84 19) 2-chloronaphthalene 16.36 162 428035 16.15 ug/L 98 20) Dimethylphthalate 17.46 163 615940 16.35 ug/L 97 21) 2,6-Dinitrotoluene 17.56 165 100363 13.68 ug/L 99 22) Acenaphthylene 17.55 152 641999. 13.25 ug/L 98 23) Acenaphthene 18.08 153 522325 17.05 ug/L 99 24) 2,4-Dinitrotoluene 18.71 165 92938 10.52 ug/L 95 25) Diethylphthalate 19.58 149 599306 19.16 ug/L 99 26) 4-Chlorophenyl-phenyl ethe 19.75 204 252519 14.60 ug/L 98 27) Fluorene 19.61 166 622492 17.61 ug/L 98 29) Azobenzen/ 1,2-Diphenylhyd 20.20 77 799743 14.70 ug/L 97 31) N-Nitrosodiphenylamine 20.12 169 296299 14.81 ug/L 98 32) 4-Bromophenyl-phenyl ether 21.18 248 125315 14.44 ug/L 90 33) Hexachlorobenzene 21.19 284 133198 16.41 ug/L 90 34) Phenanthrene 22.40 178 872940 16.79 ug/L 99 35) Anthracene 22.56 178 772458 14.56 ug/L 97 36) Di-n-butylphthalate 24.51 149 1015375 17.08 ug/L 99 37) Fluoranthene 25.90 202 854044 15.49 ug/L 84 40) Pyrene 26.53 202 966008 17.26 ug/L 88 41) Butylbenzylphthalate 28.90 149 407841 15.77 ug/L 90 42) Benzo (a) antracene 30.12 228 688982 15.24 ug/L 99 43) Bis (2-ethylhexyl) phthala 30.77 14 9 706006 19.22 ug/L 99 44) Chrysene 30.22 228 721456 16.12 ug/L 100

(#) = qualifier out of range (m) = manual integration REFA0418.D 5080402BBC.M Wed Apr 24 08:25:47 2002 Page 1

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