GCMS raw data printout for sample AE05909, March 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) d 6 Data File : C:\MSDCHEM\l\DATA\031702\3915RE.D Vial: 24 “ Acq Oh : 18 Mar 2002 5:12 am Operator: McLean Sample : 3/14/02RE EXT Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: BENZO.P Quant Time: Mar 20 11:26:52 2002 Quant Results File: 5080302.RES

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Last Update : Thu Mar 14 13:02:27 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 9.54 150 1427081 20.00 ug/L 0.00 10) Naphthalene-d8 13.03 136 3877761 20.00 ug/L 0.00 17) Acenaphthene-diO 18.13 164 2170052 20.00 ug/L 0.00 29) Phenanthrene-diO 22.50 188 3289709 20.00 ug/L 0.00 38) Chrysene-dl2 30.30 240 2998245 20.00 ug/L -0.02 44) Perylene-dl2 34.18 264 1625220 20.00 ug/L 0.00

System Monitoring Compounds 37) 2,4-ddd surr 27.44 235 301297 7.68 ug/L 0.00 Spiked Amount 5.000 Recovery = 153.60%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. d 3) bis(2-chloroethyl) ether 0.00 93 0 N.D. 4) 1,3 - Dichlorobenze 0.00 146 0 N.P 5) 1,4 - Dichlorobenzene 0.00 146 0 6) 1,2 - Dichlorobenzene 0.00 146 0 7) 2,2 ' - oxybis (l-Chloropr 0.00 45 8) N-Nitroso-di-n-propylamine 0.00 70 9) Hexachloroethane 0.00 117 11) Nitrobenzene 12) Isophorone 0.00 0 . Of' 0 13) bis(2-Chloroethoxy) methan 14) 1,2,4-Trichlorobenzene 15) Naphthalene X J 16) Hexachlorobutadiene 18) Hexachlorocyclor'

W r 19) 2-chloronapht‘ 20) 21) 22) Dimethylph 2,6-Din. Acenapht. U/N 23) Acenaphth. 24) 2,4-Dinitr 25) Diethylphth 26) 4-Chlorophen 27) Fluorene 28) Azobenzen/ 1,2 30) N-Nitrosodiphen 31) 4-Bromophenyl-ph N.D. 32) Hexachlorobenzene N.D. 33) Phenanthrene J N.D. 34) Anthracene 0 N.D. 35) Di-n-butylphthalate 0 N.D. d 36) Fluoranthene .2 0 N.D. 39) Pyrene 202 0 N.D. 40) Butylbenzylphthalate J.00 149 0 N.D. 41) Benzo (a) antracene 0.00 228 0 N.D. d 42) Bis (2-ethylhexyl) phthala 0.00 149 0 N.D. d 43) Chrysene 0.00 228 0 N.D. d 45) Di-n-Octylphthalate 0.00 149 0 N.D. 46) Benzo (b) fluoranthene 0.00 252 0 N.D.

(#) = qualifier out of range (m) = manual integration 3915RE.D 5080302.M Wed Mar 20 11:27:52 2002 Page 1

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