NYC-WTC_000039136
GCMS scan report for sample AE05910 listing results for unknown compounds analyzed on March 21, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗Document / 8 pages
GCMS analysis comments for sample AE03915, March 2002
Machine-extracted title · confidence 100%Laboratory notes for sample AE03915 documenting low surrogate recovery and subsequent re-extraction and re-analysis on March 21, 2002.
NYC-WTC_000039175–000039182Folder label: “GCMS X 3/14/02 A 3/17/02”
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NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed) 7 • Data File : C:\MSDCHEM\l\DATA\031702\3915RE.D Vial: 24 Acq On : 18 Mar 2002 5:12 am Operator: McLean Sample : 3/14/02RE EXT Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: BENZO.P Quant Time: Mar 20 11:26:52 2002 Quant Results File: 5080302.RES
Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Last Update : Thu Mar 14 13:02:27 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 9.54 150 1427081 20.00 ug/L 0.00 10) Naphthalene-d8 13.03 136 3877761 20.00 ug/L 0.00 17) Acenaphthene-diO 18.13 164 2170052 20.00 ug/L 0.00 29) Phenanthrene-diO 22.50 188 3289709 20.00 ug/L 0.00 38) Chrysene-dl2 30.30 240 2998245 20.00 ug/L -0.02 44) Perylene-dl2 34.18 264 1625220 20.00 ug/L 0.00
System Monitoring Compounds 37) 2,4-ddd surr 27.44 235 301297 7.68 ug/L 0.00 Spiked Amount 5.000 Recovery = 153.60%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. d 3) bis(2-chloroethyl) ether 0.00 93 0 N.D. 4) 1,3 - Dichlorobenze 0.00 146 0 N.D. 5) 1,4 - Dichlorobenzene 0.00 146 0 N.D. 6) 1,2 - Dichlorobenzene 0.00 146 0 N.D. 7) 2,2 1 - oxybis (l-Chloropr 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy) methan 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 0.00 128 0 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 22) Acenaphthylene 0.00 152 0 N.D. 2 3) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 0.00 149 0 N.D. 26) 4-Chlorophenyl-phenyl ethe 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. 30) N-Nitrosodiphenylamine 0.00 169 0 N.D. 31) 4-Bromophenyl-phenyl ether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 3 3) Phenanthrene 0.00 178 0 N.D. 34) Anthracene 0.00 178 0 N.D. 35) Di-n-butylphthalate 0.00 149 0 N.D. d 36) Fluoranthene 0.00 202 0 N.D. 3 9) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo (a) antracene 0.00 228 0 N.D. d 42) Bis (2-ethylhexyl) phthala 0.00 149 0 N.D. d 43) Chrysene 0.00 228 0 N.D. d 45) Di-n-Octylphthalate 0.00 149 0 N.D. 46) Benzo (b) fluoranthene 0.00 252 0 N.D.
(#) = qualifier out of range (m) = manual integration 3915RE.D 5080302.M Wed Mar 20 11:27:52 2002 Page 1
NYC-WTC_000039176
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NYC-WTC_000039176Source: NYC Law Department, mirrored locally
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