GCMS analysis results, sample AE06271, March 2002

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Gas chromatography-mass spectrometry analysis of sample AE06271 performed March 22, 2002, detecting unknown compounds and 2,4-DDD surrogate at 5.0 ug/L.

NYC-WTC_000039262–000039269

Folder label: “GCMS X 3/15/02 A 3/16/02”

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed.)

Data File : C:\MSDCHEM\l\DATA\031602\06271.D Vial: 9 Acq On : 16 Mar 2002 3:48 pm Operator: McLean Sample : 3/15 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: BENZO.P Quant Time: Mar 20 06:35:27 2002 Quant Results File: 5080302.RES

Quant Method : C:\MSDCHEM\l\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Last Update : Thu Mar 14 13:02:27 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 9.54 150 1514868 20.00 ug/L 0.00 10) Naphthalene-d8 13.03 136 4125338 20.00 ug/L 0.00 17) Acenaphthene-diO 18.13 164 2266165 20.00 ug/L 0.00 29) Phenanthrene-dlO 22.50 188 3517042 20.00 ug/L 0.00 38) Chrysene-dl2 30.31 240 3202462 20.00 ug/L 0.00 44) Perylene-dl2 34.19 264 1827116 20.00 ug/L 0.00

System Monitoring Compounds 37) 2,4-ddd surr 27.43 235 305323 7.28 ug/L 0.00 Spiked Amount 5.000 Recovery = 145.60%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. d 3) bis(2-chloroethyl) ether 0.00 93 0 N.D. 4) 1,3 - Dichlorobenze 0.00 146 0 N.D. 5) 1,4 - Dichlorobenzene 0.00 146 0 N.D. 6) 1,2 - Dichlorobenzene 0.00 146 0 N.D. 7) 2,2 1 - oxybis (l-Chloropr 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy) methan 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 0.00 128 0 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 0.00 149 0 N.D. 26) 4-Chlorophenyl-phenyl ethe 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. 30) N-Nitrosodiphenylamine 0.00 169 0 N.D. 31) 4-Bromophenyl-phenyl ether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 3 3) Phenanthrene 0.00 178 0 N.D. 34) Anthracene 0.00 178 0 N.D. 35) Di-n-butylphthalate 0.00 14 9 0 N.D. d 36) Fluoranthene 0.00 202 0 N.D. 39) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo (a) antracene 0.00 228 0 N.D. d 42) Bis (2-ethylhexyl) phthala 0.00 149 0 N.D. d 43) Chrysene 0.00 228 0 N.D. d 45) Di-n-Octylphthalate 0.00 149 0 N.D. 46) Benzo (b) fluoranthene 0.00 252 0 N.D.

(#) = qualifier out of range (m) = manual integration 06271.D 5080302.M Wed Mar 20 06:36:36 2002 Page 1

NYC-WTC_000039264

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