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GCMS unknowns report for sample AE02460, March 2002

Machine-extracted title · confidence 90%

Laboratory report detailing analysis of unknown compounds and surrogate recovery for sample AE02460.

NYC-WTC_000038801–000038816

Folder label: “GCMS X 3/4/02 A 3/20/02

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NYC 9/11 Public Portal Document yUCIIU A\CDUL 1 I V -L — WW/

Data File : C:\HPCHEM\1\DATA\MAR1902\2460.D Vial: 19 Acq On : 20 Mar 2002 10:44 pm Operator: Sample : gc/ms scan 3/4 fb Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 21 13:50 2002 <Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 08 08:54:27 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 33) Phenanthrene 25.66 178 518 N.D. 34) Anthracene 25.66 178 518 N.D. 35) Di-n-butylphthalate 27.63 149 4965 N.D. 36) Fluoranthene 0.00 202 0 N.D. 3 9) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo(a)anthracene 33.72 228 2808 N.D. 42) Bis(2-ethylhexyl)phthalate 33.93 149 1428 N.D. 43) Chrysene 33.79 228 889 N.D. 45) Di-n-Octylphthalate 35.67 149 506 N.D. 46) Benzo(b)fluoranthene 36.84 252 1770 N.D. 47) Benzo(k)fluoranthene 36.84 252 833 N.D. 48) Benzo(a)pyrene 37.78 252 610 N.D. 49) Indeno(1,2,3-cd)pyrene 42.14 276 183 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 43.34 276 294 N.D.

(#) = qualifier out of range (m) = manual integration 2460.D GCMS0308.M Thu Mar 21 13:53:12 2002 Page 2

NYC-WTC_000038804

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NYC-WTC_000038804Source: NYC Law Department, mirrored locally

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