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GCMS quantitation results for sample AE04030, March 2002

Machine-extracted title · confidence 95%

Quantitation report listing response data for deuterated internal standards and surrogates from a March 29, 2002 analysis.

NYC-WTC_000038532–000038541

Folder label: “GCMS X 2/25/02 A 3/23/02

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NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\l\DATA\MAR2202\4030.D Vial: 36 Acq On : 24 Mar 2002 4:37 am Operator: Sample : gc/ms scan 2/25 Inst : GC/MS 2 09 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 2610:162002 ।Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 08 08:54:27 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 • N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 33) Phenanthrene 0.00 178 0 N.D. d 34) Anthracene 0.00 178 0 N.D. d 35) Di-n-butylphthalate 27.62 149 11528 N.D. 36) Fluoranthene 0.00 202 0 N.D. 39) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo(a)anthracene 33.72 228 2187 N.D. 42) Bis(2-ethylhexyl)phthalate 33.93 149 27815 0.80 ug/1 # 90 43) Chrysene 33.72 228 2187 N.D. 45) Di-n-Octylphthalate 0.00 149 0 N.D. 46) Benzo(b)fluoranthene 36.78 252 171 N.D. 47) Benzo(k)fluoranthene 0.00 252 0 N.D. 48) Benzo(a)pyrene 37.97 252 1983 N.D. 49) Indeno(1,2,3-cd)pyrene 0 . OCt 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 4030 .D GCMS0308.M Tue Mar 26 10:17:34 2002 Page 2

NYC-WTC_000038535

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NYC-WTC_000038535Source: NYC Law Department, mirrored locally

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