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GCMS analysis results for sample AE01440, Mar 2002

Machine-extracted title · confidence 100%

Gas chromatography-mass spectrometry analysis report for environmental sample AE01440 dated March 29, 2002.

NYC-WTC_000038613–000038622

Folder label: “GCMS X 2/25/02 A 3/23/02

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NYC 9/11 Public Portal Document ACDOL

Data File : C:\HPCHEM\1\DATA\MAR2202\1440.D Vial: 43 Acq On : 24 Mar 2002 11:32 am Operator: Sample : re-extract Inst : GC/MS 2 09 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 12.267 781 787 801 rVB 1068734 2502075 66.30% 13.074% 2 14.865 1065 1070 1075 rBV 68102 133262 3.53% 0.696% 3 15.903 1177 1183 1200 rBV 1668384 3355550 88.92% 17.534% 4 21.209 1755 1761 1786 rBV 1800469 3769892 99.90% 19.699% 5 25.661 2239 2246 2256 rBV2 1684784 3773612 100.00% 19.718%

6 25.790 2257 2260 2273 rVB 15176 46562 1.23% 0.243% 7 27.626 2454 2460 2465 rBV 38754 76253 2.02% 0.398% 8 30.729 2793 2798 2805 rVB 216758 424392 11.25% 2.218% 9 33.722 3116 3124 3141 rBV2 1239519 2865136 75.93% 14.971% 10 33.933 3141 3147 3160 rVB 93350 213451 5.66% 1.115%

11 37.972 3578 3587 3607 rBV2 672123 1977670 52.41% 10.334%

Sum of corrected areas: 19137855

1440.D GCMS0308.M Tue Mar 26 10:39:54 2002

NYC-WTC_000038618

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NYC-WTC_000038618Source: NYC Law Department, mirrored locally

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