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GCMS analysis results for sample AE01440, Mar 2002

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Gas chromatography-mass spectrometry analysis report for environmental sample AE01440 dated March 29, 2002.

NYC-WTC_000038613–000038622

Folder label: “GCMS X 2/25/02 A 3/23/02

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NYC 9/11 Public Portal Document LSDV VL KEveweC)

* Data File : C:\HPCHEM\1\DATA\MAR2202\1440.D Vial: 43 Acq On : 24 Mar 2002 11:32 am Operator: Sample : re-extract Inst : GC/MS 2 09 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 2610:292002 <Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 08 08:54:27 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 ' N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 33) Phenanthrene 25.65 178 508 N.D. 34) Anthracene 25.65 178 508 N.D. 35) Di-n-butylphthalate 27.62 149 46659 0.57 ug/1 98 36) Fluoranthene 0.00 202 0 N.D. 39) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo(a)anthracene 33.71 228 2237 N.D. 42) Bis(2-ethylhexyl)phthalate 33.93 149 62452 1.58 ug/1 # 92 43) Chrysene 33.71 228 2237 N.D. 45) Di-n-Octylphthalate 0.00 149 0 N.D. 46) Benzo(b)fluoranthene 0.00 252 0 N.D. 47) Benzo(k)fluoranthene 0.00 252 0 N.D. 48) Benzo(a)pyrene 37.96 252 2133 N.D. 49) Indeno(1,2,3-cd)pyrene 0.00- 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 1440.D GCMS0308,M Tue Mar 26 10:30:59 2002 Page 2

NYC-WTC_000038616

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NYC-WTC_000038616Source: NYC Law Department, mirrored locally

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