GCMS analysis results for sample AE01440, Mar 2002

NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\l\DATA\MAR2202\1440.D Vial: 43 Acq On : 24 Mar 2002 11:32 am Operator: Sample : re-extract Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 26 10:29 2002 iQuant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 08 08:54:27 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.27 152 456418 ■ 20.00 ug/1 -0.09 10) Naphthalene-d8 15.90 136 1777923 20.00 ug/1 -0.10 17) Acenaphthene-diO 21.21 164 980077 20.00 ug/1 -0.10 29) Phenanthrene-diO 25.65 188 1495972 20.00 ug/1 -0.11 38) Chrysene-dl2 33.72 240 988694 20.00 ug/1 -0.12 44) Perylene-dl2 37.97 264 580320 20.00 ug/1 -0.15

System Monitoring Compounds 5. 30 37) 2,4-DDD 30.73 235 87859 8.08ug/mL 0.23 Spiked Amount 5.000 Recovery 161.60% /077o Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) his(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0 .00- 146 0 N.D. 7) 2,21-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Is ophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 18 0 0 N.D. 15) Naphthalene 0.00 128 0 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.69 149 398 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.

(#) = qualifier out of range (m) = manual integration 1440 .D GCMS0308.M Tue Mar 26 10:30:55 2002 Page 1

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