NYC 9/11 Public Portal Document
Data File : C:\HPCHEM\l\DATA\MAR2202\4031.D Vial: 37
Acq On : 24 Mar 2002 5:36 am Operator:
Sample : gc/ms scan 2/25 fb Inst : GC/MS 209
Mise : Multiplr: 1.00
MS Integration Params: GOOFY.P
Quant Time: Mar 2610:182002 <Quant Results File: GCMS0308.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Last Update : Fri Mar 08 08:54:27 2002
Response via : Initial Calibration
DataAcq Meth : GCMS0308
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 12.27 152 440407 ■ 20.00 ug/1 -0.09
10) Naphthalene-d8 15.90 136 1761048 20.00 ug/1 -0.10
17) Acenaphthene-diO 21.21 164 966412 20.00 ug/1 -0.11
29) Phenanthrene-dlO 25.66 188 1446140 20.00 ug/1 -0.11
38) Chrysene-dl2 33.72 240 933140 20.00 ug/1 -0.12
44) Perylene-dl2 37.97 264 575823 20.00 ug/1 -0.15
System Monitoring Compounds
37) 2,4-DDD 30.73 235 88544
5
-8—42 ug/mL 0.23
Spiked Amount
Target Compounds
5.000 Recovery 168.
/o T
Qvalue
2) N-nitroso-dimethyl amine 5.48 74 201 N.D.
3) bis(2-Chloroethyl)ether 0.00 93 0 N.D.
4) 1,3-Dichlorobenzene 0.00 146 0 N.D.
5) 1,4-Dichlorobenzene 0.00 146 0 N.D.
6) 1,2-Dichlorobenzene 0.00- 146 0 N.D.
7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D.
8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D.
9) Hexachloroethane 0.00 117 0 N.D.
11) Nitrobenzene 0.00 77 0 N.D.
12) is ophorone 0.00 82 0 N.D.
13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D.
14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D.
15) Naphthalene 15.95 128 285 N.D.
16) Hexachlorobutadiene 0.00 225 0 N.D.
18) Hexachlorocyclopentadiene 0.00 237 0 N.D.
19) 2-Chloronaphthalene 0.00 162 0 N.D.
20) Dimethylphthalate 0.00 163 0 N.D.
21) 2,6-Dinitrotoluene 0.00 165 0 N.D.
22) Acenaphthylene 0.00 152 0 N.D.
23) Acenaphthene 0.00 153 0 N.D.
24) 2,4-Dinitrotoluene 0.00 165 0 N.D.
25) Diethylphthalate 22.70 149 159 N.D.
26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D.
27) Fluorene 0.00 166 0 N.D.
28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration
4031.D GCMS0308.M Tue Mar 26 10:19:28 2002 Page 1
NYC-WTC_000038544
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