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GCMS analysis results for sample AE03914, Mar 18 2002

Machine-extracted title · confidence 50%

Laboratory report documenting GCMS analysis of sample AE03914 for unknown compounds on March 18, 2002.

NYC-WTC_000038352–000038363

Folder label: “GCMS X 2/22/02 A 2/24/02

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Scanned page image, NYC-WTC_000038357
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document LSC area Percent Keporc

Data File : C:\HPCHEM\1\DATA\FEB2102\3914.D Vial: 76 ' Acq On : 24 Feb 2002 8:48 pm Operator: Sample : gc/ms scan 2/22 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.204 339 344 357 rBV 79227 210395 10.81% 2.083% 2 9.269 454 460 464 rBV 8833 19541 1.00% 0.193% 3 12.326 788 793 809 rBV 545920 1376481 70.71% 13.626% 4 15.971 1184 1190 1206 rBV 868128 1816485 93.31% 17.982% 5 21.176 . 1752 1757 1763 rBV 16569 33768 1.73% 0.334%

6 21.286 1763 1769 1792 rW 922489 1946640 100.00% 19.270% 7 25.729 2247 2253 2265 rBV2 850522 1864004 95.75% 18.452% 8 25.876 2265 2269 2282 rVB3 7362 22680 1.17% 0.225% 9 30.806 2799 2806 2813 rBV 108557 213393 10.96% 2.112% 10 33.799 3125 3132 3152 rBV2 640594 1484104 76.24% 14.691%,

11 38.077 3590 3598 3617 rBV2 347182 1114310 57.24% 11.031%

Sum of corrected areas: 10101801

3914.D GCMS0208.M Wed Mar 13 11:35:45 2002

NYC-WTC_000038357

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NYC-WTC_000038357Source: NYC Law Department, mirrored locally

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