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GCMS analysis results for sample AE04024, Mar 15 2002

Machine-extracted title · confidence 50%

Laboratory report documenting GCMS analysis of sample AE04024 conducted on March 15, 2002.

NYC-WTC_000038302–000038313

Folder label: “GCMS X 2/22/02 A 2/24/02

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Scanned page image, NYC-WTC_000038307
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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\FEB2102\4024.D Vial: 79 Acq On : 24 Feb 2002 11:45 pm Operator: Sample : gc/ms scan 2/22 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height. area % max. total

1 8.201 340 344 355 rBV 98965 246351 12.67% 2.514% 2 8.311 355 356 367 rVB2 11233 21072 1.08% 0.215% 3 12.332 788 794 809 rVB 560293 1360565 69.97% 13.884% 4 15.968 1184 1190 1208 rBV 830656 1784729 91.78% 18.213% 5 21.173 1753 1757 1763 rBV 13401 25782 1.33% 0.263%

6 21.283 1763 1769 1786 rBV 932079 1944487 100.00% 19.843% 7 25.726 2247 2253 2265 rBV2 807203 1789310 92.02% 18.259% 8 25.873 2265 2269 2278 rVB2 6869 20533 1.06% 0.210% 9 30.812 2801 2807 2814 rVB 126990 263996 13.58% 2.694%, 10 33.796 3126 3132 3148 rBV2 583459 1348401 69.34% 13.760%

11 38.074 3590 3598 3616 rBV2 317257 994127 51.13% 10.145%

Sum of corrected areas: 9799353

4024.D GCMS0208.M Wed Mar 13 11:38:46 2002

NYC-WTC_000038307

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NYC-WTC_000038307Source: NYC Law Department, mirrored locally

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