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GCMS analysis results for sample AE03914, Mar 18 2002

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Laboratory report documenting GCMS analysis of sample AE03914 for unknown compounds on March 18, 2002.

NYC-WTC_000038352–000038363

Folder label: “GCMS X 2/22/02 A 2/24/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\FEB2102\3914.D Vial: 76 Acq On : 24 Feb 2002 8:48 pm Operator: Sample : gc/ms scan 2/22 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 13 11:17 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 27 11:30:15 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 33) Phenanthrene 0.00 178 0 N.D. 34) Anthracene 0.00 178 0 N.D. 35) Di-n-butylphthalate 27.70 14 9 906 N.D. 36) Fluoranthene 0.00 202 0 N.D. 39) Pyrene 0 : 00 202 0 N.D. 40) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo(a)anthracene 33.80 228 1030 N.D. 42) Bis(2-ethylhexyl)phthalate 34.01 149 731 N.D. 43) Chrysene 33.80 228 1029 N.D. 45) Di-n-Octylphthalate 0.00 149 0 N.D. 46) Benzo(b)fluoranthene 0.00 252 0 N.D. 47) Benzo(k)fluoranthene 0.00 252 0 N.D. 48) Benzo(a)pyrene 3 8.08 252 ■ 1375 N.D. 49) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 3914 .D GCMS0208.M Wed Mar 13 11:18:34 2002 Page 2

NYC-WTC_000038355

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NYC-WTC_000038355Source: NYC Law Department, mirrored locally

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