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GCMS analysis results, sample AE04026, March 2002

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Gas chromatography-mass spectrometry analysis report for sample AE04026, completed March 15, 2002, identifying unknown compounds and surrogate recovery data.

NYC-WTC_000038324–000038333

Folder label: “GCMS X 2/22/02 A 2/24/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\FEB2102\4026.D Vial: 81 Acq On : 25 Feb 2002 1:42 am Operator: Sample : gc/ms scan 2/22 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 13 11:26 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 27 11:30:15 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. .31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 33) Phenanthrene 0.00 178 0 N.D. 34) Anthracene 0.00 178 0 N.D. 35) Di-n-butylphthalate 27.70 149 1440 N.D. 36) Fluoranthene 0.00 202 .0 N.D. 39) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo(a)anthracene 33.80 228 1103 N.D. 42) Bis(2-ethylhexyl)phthalate 34.02 149 1106 N.D. 43) Chrysene 33.80 228 1103 N.D. 45) Di-n-Octylphthalate 0.00 149 0 N.D. 46) Benzo(b)fluoranthene 0.00 252 0 N.D. 47) Benzo(k)fluoranthene 0.00 252 0 N.D. 48) Benzo(a)pyrene 38.07- 252 1066 N.D. 49) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 4026.D GCMS0208.M Wed Mar 13 11:27:17 2002 Page 2

NYC-WTC_000038327

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NYC-WTC_000038327Source: NYC Law Department, mirrored locally

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