GCMS analysis results for sample AE03914, Mar 18 2002

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Laboratory report documenting GCMS analysis of sample AE03914 for unknown compounds on March 18, 2002.

NYC-WTC_000038352–000038363

Folder label: “GCMS X 2/22/02 A 2/24/02”

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\FEB2102\3914.D Vial: 76 Acq On : 24 Feb 2002 8:48 pm Operator: Sample : gc/ms scan 2/22 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 13 11:17 2002 (Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb. 27 11:30:15 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Internal Standards R.T. Qlon- Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.34 152 236478 20.00 ug/1 -0.02 10) Naphthalene-d8 15.97 136 925145 20.00 ug/1 -0.03 17) Acenaphthene-diO 21.29 164 491523 20.00 ug/1 -0.03 29) Phenanthrene-dlO 25.73 188 702469 20.00 ug/1 -0.04 38) Chrysene-dl2 33.80 240 484105 20.00 ug/1 -0.05 44) Perylene-dl2 38.08 264 313730 20.00 ug/1 -0.05

System Monitoring Compounds 37) 2,4-DDD 30.81 235 40315 5.50ug/mL 0.31 Spiked Amount 5.000 Recovery = 110.00%

Target Compounds 66’0Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,21-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 0.00 128 0 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 ' 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 2 2) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.77 149 200 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.

(#) = qualifier out of range (m) = manual integration 3914 .D GCMS0208.M Wed Mar 13 11:18:30 2002 Page 1

NYC-WTC_000038354

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GCMS analysis results for sample AE03915, Mar 18 2002 · Box DEP Box 23

NYC-WTC_000038342

Laboratory report documenting GCMS analysis of sample AE03915 for unknown compounds on March 18, 2002.

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