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GCMS blank analysis results, sample AE03833, Mar 13 2002

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Laboratory report documenting GCMS blank analysis for sample AE03833 conducted on March 13, 2002.

NYC-WTC_000038265–000038272

Folder label: “GCMS X 2/22/02 A 2/24/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\FEB2102\LBE.D ■ Vial: 70 Acq On : 24 Feb 2002 2:55 pm Operator: Sample : gc/ms scan 2/22 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 13 11:05 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 27 11:30:15 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 24.82 284 433 N.D. 33) Phenanthrene 25.80 178 . 2347 N.D. 34) Anthracene 25.80 178 2347 N.D. 35) Di-n-butylphthalate 27.71 149 1922 N.D. 36) Fluoranthene 29.43 202 1643 N.D. 39) Pyrene 30.11 202 1991 N.D. 40) Butylbenzylphthalate 32.23 149 786 N.D. 41) Benzo(a)anthracene 33.75 228 4077 N.D. 42) Bis(2-ethylhexyl)phthalate 34.01 149 1531 N.D. 43) Chrysene 33.88 228 3598 N.D. 45) Di-n-Octylphthalate 35.74 149 436 N.D. 46) Benzo(b)fluoranthene 36.88 252 1434 N.D. 47) Benzo(k)fluoranthene 36.95 252 2324 N.D. 48) Benzo(a)pyrene 37.88 252 868 N.D. 49) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration LBE.D GCMS0208.M Wed Mar 13 11:06:36 2002 Page 2

NYC-WTC_000038267

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NYC-WTC_000038267Source: NYC Law Department, mirrored locally

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