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GCMS analysis results for sample AD31591, Feb 28 2002

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Laboratory report documenting GCMS analysis of sample AD31591 conducted on February 28, 2002.

NYC-WTC_000038205–000038219

Folder label: “GCMS X 2/21/02 A 2/22/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\FEB2102\31591.D Vial: 38 Acq On : 23 Feb 2002 3:36 am Operator: Sample : gc/ms scan 2/21 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 27 11:45 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 27 11:30:15 2.002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 24.40 248 225 N.D. 32) Hexachlorobenzene 24.83 284 333 N.D. 33) Phenanthrene 25.80 178 2632 N.D. 34) Anthracene 25.92 178 1034 N.D. 35) Di-n-butylphthalate 27.69 149 2726 N.D. 36) Fluoranthene 29.44 202 1623 N.D. 39) Pyrene 30.11 202 1992 N.D. 40) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo(a)anthracene 33.81 228 1309 N.D. 42) Bis(2-ethylhexyl)phthalate 34.01 149 6401 N.D. 43) Chrysene 33.81 228 1309 N.D. 45) Di-n-Octylphthalate 0.00 149 0 N.D. 46) Benzo(b)fluoranthene 0.00 252 0 N.D. 47) Benzo(k)fluoranthene 0.00 252 0 N.D. 48) Benzo(a)pyrene 38.09 252 1391 N.D. 49) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 31591.D GCMS0208.M Wed Feb 27 11:46:04 2002 Page 2

NYC-WTC_000038208

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NYC-WTC_000038208Source: NYC Law Department, mirrored locally

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