NYC 9/11 Public Portal Document
tc11t. —C \ 2X IS V —LwCw/
Data File : C:\HPCHEM\1\DATA\FEB2102\LBE.D Vial: 70
Acq On : 24 Feb 2002 2:55 pm Operator:
Sample : gc/ms scan 2/22 Inst : GC/MS 209
Mise : Multiplr: 1.00
MS Integration Params: GOOFY.P
Quant Time: Mar 13 11:05 2002 Quant Results File: GCMS0208.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Last Update : Wed Feb 27 11:30:15 2002
Response via : Initial Calibration
DataAcq Meth : GCMS0208
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 12.33 152 213411 - 20.00 ug/1 -0.02
10) Naphthalene-d8 15.97 136 820238 20.00 ug/1 -0.02
17) Acenaphthene-diO 21.28 164 433959 20.00 ug/1 -0.03
29) Phenanthrene-diO 25.73 188 595320 20.00 ug/1 -0.03
38) Chrysene-dl2 33.80 240 374135 20.00 ug/1 -0.04
44) Perylene-dl2 38.07 264 224639 20.00 ug/1 -0.05
System Monitoring Compounds J 66
37) 2,4-DDD 30.81 235 43185 6-95 ug/mL 0.31
Spiked Amount 5,000 Recovery 139.00%
176
Target Compounds Qvalue
2) N-nitroso-dimethyl amine 5.97 74 420 N.D.
3) bis(2-Chloroethyl)ether 11.72 93 726 N.D.
4) 1,3-Dichlorobenzene 12.23 146 681 _ N.D.
5) 1,4-Dichlorobenzene 12.38 146 971 N.D.
6) 1,2-Dichlorobenzene 12.90 146 630 N.D.
7) 2,21-oxybis(1-Chloropropan 0.00 45 0 N.D.
8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D.
9) Hexachloroethane 13.74 117 100 N.D.
11) Nitrobenzene 14.01 77 516 N.D.
12) Isophorone 14.69 82 1007 N.D.
13) bis(2-Chloroethoxy)methane 15.35 93 280 N.D.
14) 1,2,4-Trichlorobenzene 15.85 180 528 N.D.
15) Naphthalene 16.03 128 2700 N.D.
16) Hexachlorobutadiene 16.57 225 316 N.D.
18) Hexachlorocyclopentadiene 0.00 237 0 N.D.
19) 2-Chloronaphthalene 19.55 162 1114 N.D.
20) Dimethylphthalate 20.65 163 1272 N.D.
21) 2,6-Dinitrotoluene 0.00 165 0 N.D.
22) Acenaphthylene 20.81 152 1467 N.D.
23) Acenaphthene 21.38 153 1645 N.D.
24) 2,4-Dinitrotoluene 0.00 165 0 N.D.
25) Diethylphthalate 22.76 149 1413 N.D.
26) 4-Chlorophenyl-phenylether 22.92 204 406 N.D.
27) Fluorene 22.91 166 1343 N.D.
28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration
LBE.D GCMS0208.M Wed Mar 13 11:06:33 2002 Page 1
NYC-WTC_000038266
OCR can misread numbers and units. Confirm readings against the page image before using them.