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GCMS analysis results for sample AD31588, Feb 28 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD31588 conducted on February 28, 2002.

NYC-WTC_000038196–000038204

Folder label: “GCMS X 2/21/02 A 2/22/02

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Scanned page image, NYC-WTC_000038201
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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\l\DATA\FEB2102\31588.D Vial: 41 Acq On 23 Feb 2002 6:33 am Operator: Sample gc/ms scan 2/21 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0. Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal . : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.195 339 343 359 rBV 121688 321801 14.02% 2.770% 2 12.335 788 794 807 rVB 675438 1644115 71.63% 14.154% 3 15.970 1184 1190 1207 rBV 1025348 2164074 94.28% 18.631% 4 21.286 1763 1769 1788 rBV 1122885 2295395 100.00% 19.761% 5 25.738 2247 2254 2265 rBV2 988624 2167097 94.41% 18.657%

6 30.815 2802 2807 2813 rBV 128232 260990 11.37% 2.247% 7 33.798 3126 3132 3152 rBV2 669630 1583179 68.97% 13.630% 8 38.086 3590 3599 3616 rBV2 371233 1178895 51.36% 10.149%

Sum of corrected areas: 11615546

31588.D GCMS0208.M Wed Feb 27 12:03:03 2002

NYC-WTC_000038201

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NYC-WTC_000038201Source: NYC Law Department, mirrored locally

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