GCMS analytical results for sample AE03832, March 29, 2002

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Data File : C:\HPCHEM\l\DATA\MAR2202\3832.D Vial: 13 Acq On : 23 Mar 2002 5:55 am Operator: Sample : gc/ms scan 2/20 fb Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Cyclopentasiloxane, decamethyl Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

14.87 0.81 ug/1 115953 Naphthalene-d8 15.90

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 90 2 3,4 -Dihydroxybenzyl alcohol, tris (tr 356 C16H3203Si3 068595-79-9 49 3 N-(Trifluoroacetyl)-N, O, OO 1 '-tetr 55.3 C22H42F3NO4Si4 000000-00-0 47 4 Benz eneethanami ne, N - [ (pent a f l uorop 56 3 C2 4H34F5NO3Si3 055429-13-5 3 2 Abundance Scan 1070 (14.866 min). 3832.D (-) m/z 73.0,0 100.00% 73 ft 5000 - 267 355

.................. /............. 45 323 14.60 14.80 15.00 15.20 125 154 193 223 , — ------- TAI-T m/z 355.05 48.55% miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 5000- 14.60 14.80 15.00 15.20 m/ Z 267.00 45.60% ...... 207 , 323 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #49868: 3,4-Dihydroxybenzyl alcohol, tris(trimethylsilyl)- 73 T‘/ IF 14.60 14.80 15.00 15.20 267 5000 179 m/ z 356.05 17.45% 356 45 147 ........ , 209 237 312 ....................... ' 1 1 I m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60162: N-(Trifluoroacetyl)-N,O,O’,O''-tetrakis(trimethylsi IT ■ i ■ ■ 73 14.60 14.80 15.00 15.2 m/ z 2 68.00 12.37% 355 5000

45 । 147 193 267 ................. 538 m/z-> 50 100 150 200 250 300 350 400 450 500 550 14.60 14.80 15.00 15.20

3832.D GCMS0308.M Tue Mar 26 15:00:09 2002 Page 1

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